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Basic Information
| CAS No.: | 925-93-9 |
|---|---|
| Name: | ETHANOL-D |
| Article Data: | 46 |
| Molecular Structure: | |
|
|
|
| Formula: | C2H5 D O |
| Molecular Weight: | 47.0611 |
| Synonyms: | Ethylalcohol-d (6CI,8CI); Ethanol (C2H5OD); Ethanol-d1; Ethanol-d1 |
| EINECS: | 213-128-9 |
| Density: | 0.78 g/cm3 |
| Melting Point: | -130 °C(lit.) |
| Boiling Point: | 72.6 °C at 760 mmHg |
| Flash Point: | 8.9 °C |
| Solubility: | complete in all proportions |
| Appearance: | colourless liquid |
| Hazard Symbols: |
 F
|
| Risk Codes: | R11 |
| Safety: | S16 S7 |
| PSA: | 20.23000 |
| LogP: | -0.00140 |
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Synthetic route
- 127022-76-8
ethoxy(diphenyl)-λ6-sulfanenitrile
A
- 925-93-9
ethyl [2]alcohol
B
- 22731-83-5
S,S-diphenylsulphoximine
Conditions
| Conditions | Yield |
|---|---|
| With [D3]acetonitrile; water-d2 In phosphate buffer at 20℃; for 0.75h; pH=6.1; Kinetics; Thermodynamic data; Product distribution; Further Variations:; pH-values; Reagents; Solvents; Temperatures; Hydrolysis; | A 86% B 99% |
Conditions
| Conditions | Yield |
|---|---|
| With triphenyl phosphine In benzene-d6; (2)H8-toluene (N2); dissolved Ir-compound with 1 drop toluene-d-8; placed in NMR tube; added triphenyl phosphine; (2)H NMR; | A n/a B 64% |
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid; water-d2 |
Conditions
| Conditions | Yield |
|---|---|
| With (CD3COCD3)D(1+) In gas at 57.9℃; Rate constant; Mechanism; Thermodynamic data; experiment conditions: NBS pulsed ion cyclotron resonance; probability of a reactive H/D exchange encounter for the deuteronated ion as a function of the Gibbs free-energy change of the (endoergic) deuteron transfer reaction; | |
| With (C2D5)2OD(1+) In gas at 57.9℃; Rate constant; Mechanism; experiment conditions: NBS pulsed ion cyclotron resonance; probability of a reactive H/D exchange encounter for the deuteronated ion as a function of the Gibbs free-energy change of the (endoergic) deuteron transfer reaction; | |
| With water-d2 In water at 34.9℃; Equilibrium constant; |
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid; water-d2 |
Conditions
| Conditions | Yield |
|---|---|
| With water-d2; decalin | |
| With diethyl ether; water-d2 | |
| With water-d2 |
Conditions
| Conditions | Yield |
|---|---|
| With decane; water-d2 | |
| With water-d2 at 80℃; |
Conditions
| Conditions | Yield |
|---|---|
| With thionyl chloride; water-d2 1.) 0 deg C, 1 h, 2.) ambient temp., 2 h, 3) reflux, 4 weeks; | 175 g |
- 74-87-3
methylene chloride
- 14621-84-2
diazomethane-d2
A
- 64-17-5
ethanol
B
- 4960-87-6
chloromethane-d2
C
- 925-93-9
ethyl [2]alcohol
D
- 1111-89-3
D3-chloromethane
Conditions
| Conditions | Yield |
|---|---|
| at -78℃; Product distribution; Irradiation; various alkylhalides; |
...Expand
- 865-49-6
chloroform-d1
- 86852-11-1, 18509-25-6
diethoxyltriphenylphosphorane
A
- 75-00-3
chloroethane
B
- 925-93-9
ethyl [2]alcohol
C
- 35976-76-2
ethyl deuterioformate
D
- 791-28-6
Triphenylphosphine oxide
Conditions
| Conditions | Yield |
|---|---|
| at 70℃; for 72h; | |
| at 70℃; for 72h; Product distribution; |
...Expand
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ETHANOL-D
