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93-44-7

Basic Information
CAS No.: 93-44-7
Name: 2-Naphthyl benzoate
Article Data: 86
Molecular Structure:
Molecular Structure of 93-44-7 (2-Naphthyl benzoate)
Formula: C17H12O2
Molecular Weight: 248.281
Synonyms: 2-Naphthalenol,benzoate (9CI);2-Naphthol, benzoate (6CI,7CI,8CI);2-Benzoyloxynaphthalene;Benzonaphthol;Betabenzon;NSC 5537;Naphthalen-2-ylbenzoate;b-Naphthyl benzoate;2-Naphthalenol,2-benzoate;
EINECS: 202-247-1
Density: 1.199 g/cm3
Melting Point: 105-109 °C
Boiling Point: 413.5 °C at 760 mmHg
Flash Point: 174.6 °C
Solubility: insoluble in water
Appearance: light brown crystalline powder
Safety: 24/25
PSA: 26.30000
LogP: 4.05900
Synthetic route
65-85-0

benzoic acid

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With TiO(acac)2 In xylene for 36h; Heating;100%
Stage #1: benzoic acid With trifluoroacetic anhydride; indium(III) chloride at 20℃;
Stage #2: β-naphthol at 20℃; for 0.166667h;
98%
With N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; triethylamine In dichloromethane for 1h; Ambient temperature;91%
98-88-4

benzoyl chloride

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
zirconium(IV) oxychloride In dichloromethane at 20℃; for 21h;98%
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere; Schlenk technique;98%
at 60℃; for 2h;97%
93-97-0

benzoic acid anhydride

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
Stage #1: benzoic acid anhydride With molybdenium(VI) dioxodichloride In dichloromethane at 20℃; for 0.5h;
Stage #2: β-naphthol In dichloromethane at 20℃; for 70h;
98%
With bismuth(lll) trifluoromethanesulfonate In acetonitrile for 0.75h; Heating;95%
With bismuth oxide perchlorate In dichloromethane at 20℃; for 1h;92%
769-78-8

vinyl benzoate

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In neat (no solvent) at 70 - 140℃; for 0.183333h; Microwave irradiation;98%
613-90-1

benzoyl cyanide

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With dmap; 1-ethylene glycol monomethyl ether-3-methylimidazolium methanesulfonate at 25 - 35℃;97%
18081-08-8

2-naphthyl trimethylsilyl ether

93-97-0

benzoic acid anhydride

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
bismuth(lll) trifluoromethanesulfonate In acetonitrile for 1.5h; Heating;95%
2797-52-6

mono-O-benzoyl maleic hydrazide

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 70 - 80℃; for 5h;95%
100-52-7

benzaldehyde

135-19-3

β-naphthol

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-1-ium chloride; palladium diacetate; sodium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 100℃; for 24h; Sealed tube;94%
With sodium cyanide; copper(l) iodide; sodium hydroxide In neat (no solvent) at 120℃; for 23h;89%
With iron(II) triflate; potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 90℃; for 24h;83%
32316-92-0

naphthalene-2-boronic acid

100-52-7

benzaldehyde

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With iron(II) triflate; potassium tert-butylate; oxygen; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 90℃; for 6h;92%
32316-92-0

naphthalene-2-boronic acid

98-88-4

benzoyl chloride

93-44-7

2-naphthyl benzoate

Conditions
ConditionsYield
With oxygen; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0) In 5,5-dimethyl-1,3-cyclohexadiene at 60℃; under 760.051 Torr; for 12h;92%
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Chemistry

IUPAC Name: Naphthalen-2-yl Benzoate
CAS:93-44-7
EINECS:202-247-1
Product Categories: Pharmaceutical Raw Materials ; Aromatic Ester ; Functional Materials ; Liquid Crystals & Related Compounds ; Phenyl Esters (Liquid Crystals).
Following is the Molecular Structure of 2-Naphthyl Benzoate (93-44-7):

SMILES: O=C(Oc2ccc1c(cccc1)c2)c3ccccc3
InChI: InChI=1/C17H12O2/c18-17(14-7-2-1-3-8-14)19-16-11-10-13-6-4-5-9-15?(13)12-16/h1-12H
InChIKey: DWJIJRSTYFPKGD-UHFFFAOYAH
Std. InChI: InChI=1S/C17H12O2/c18-17(14-7-2-1-3-8-14)19-16-11-10-13-6-4-5-9-1?5(13)12-16/h1-12H Std. InChIKey: DWJIJRSTYFPKGD-UHFFFAOYSA-N
Molecular Formula:C17H12O2
Molar Volume: 206.9cm3
Melting Point: 105-109℃
Boiling Point: 413.5℃ at 760mmHg
Flash Point: 174.6℃
Density: 1.199g/cm3
Molar Refractivity: 75.74cm3
Polarizability: 30.02 10-24cm3
Enthalpy of Vaporization: 66.63kJ/mol
Vapour Pressure: 4.77E-07mmHg at 25℃

Uses

 2-Naphthyl Benzoate (93-44-7) can be used as hardening agent for paraffin.

Safety Profile

Safety Description: S22 S24/25.
S22 Do not breathe dust.
S24 Avoid contact with skin.
S25 Avoid contact with eyes.
Ingestion: May cause irritation of the digestive tract. The toxicological properties of this substance have not been fully investigated.
Inhalation: May cause respiratory tract irritation.
Skin: May cause skin irritation.
Eyes: May cause eye irritation.

Specification

 2-Naphthyl Benzoate (93-44-7),which also can be called for Benzoic Acid 2-Naphthyl Ester ; Benzonaphthol ; Beta-Naphthyl Benzoate ; Beta-Naphthyl Benzoate ; 2 Benzoxynaphthalene ; 2-Naphthol Bezoate ; 2-Naphthyl Benzoate ; 2-Benzoyloxy Naphthalene . 2-Naphthyl Benzoate (93-44-7) is a kind of light brown crystalline powder. This chemical is stable under normal temperatures and pressures.After decomposition it turned into Carbon Monoxide and Carbon Dioxide . 2-Naphthyl Benzoate (93-44-7) should be stored in a tightly closed container of cool,dry places. When you are handling this chemical,take care of avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.