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951127-25-6

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Basic Information
CAS No.: 951127-25-6
Name: CPo3604-01
Article Data: 38
Molecular Structure:
Molecular Structure of 951127-25-6 (CPo3604-01)
Formula: C16H19F2NO4
Molecular Weight: 327.328
Synonyms: CPo3604-01;tert-butyl [(2R,3S)-5-oxo-2-(2,5-difluorophenyl)tetradihydro-2H-pyran-3-yl]carbaMate;tert-butyl [(2R,3S)-2-(2,5-difluorophenyl)-5-oxotetrahydro-2H-pvran-3 yl]carbaMate;tert-butyl ((2R,3S)-2-(2,5-difluorophenyl)-5-oxotetrahydro-2H-pyran-3-yl)carbaMate;N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-CarbaMic acid 1,1-diMethylethyl ester;Product NaMe:MK-3102 interMediate;Omarigliptin inter. OG-1;Carbamic acid, N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-, 1,1-dimethylethyl ester
EINECS: -0
Density: 1.25±0.1 g/cm3(Predicted)
Boiling Point: 433.4±45.0 °C(Predicted)
PSA: 64.63000
LogP: 3.27950
Related products
Synthetic route

C19H25F2NO5

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With hydrogenchloride In water; ethyl acetate at 20℃;95%
1172623-99-2

tert-butyl ((2R,3S)-2-(2,5-difluorophenyl)-5-hydroxytetrahydro-2H-pyran-3-yl)carbamate

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With Dess-Martin periodane In dichloromethane at 0 - 30℃; for 4h;94.7%
With Dess-Martin periodane In dichloromethane at 0 - 20℃; for 4h;94.7%
With Dess-Martin periodane In dichloromethane at 0 - 4℃; for 4h;94.7%

C19H25F2NO3S2

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With zinc(II) chloride In ethanol at 0℃; Inert atmosphere; Large scale;93.5%
951127-31-4

[(2R,3S)-5-methylene-2-(2,5-difluorophenyl)tetrahydro-2H-pyran-3-yl]carbamic acid tert-butyl ester

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With sodium periodate; ruthenium(III) chloride trihydrate In dichloromethane; water; acetonitrile at 25℃; for 3h;84%
With sodium periodate; rhodium(III) chloride
With sodium periodate; osmium(VIII) oxide In 1,4-dioxane; water at 0℃; for 2h;

tert-butyl ((8R,9S)-8-(2,5-difluorophenyl)-7-oxa-1,4-dithiaspiro[4.5]decan-9-yl)carbamate

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile at 20℃; for 1h;79%
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile at 20℃; for 0.5h;79%
With bis-[(trifluoroacetoxy)iodo]benzene In water; acetonitrile at 20℃; for 1h;79%
951127-32-5

[(2R,3S)-5-hydroxy-5-hydroxymethyl-2-(2,5-difluorophenyl)tetrahydro-2H-pyran-3-yl]carbamic acid tert-butyl ester

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
With pyridine; lead(IV) acetate In methanol for 0.333333h;
With pyridine; lead(IV) acetate In methanol at 0℃; for 0.333333h;
With pyridine; lead(IV) tetraacetate In methanol at 0℃; for 0.333333h;
35730-09-7

2,5-difluorobenzoyl chloride

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: N-ethyl-N,N-diisopropylamine
2: sodium hydride
3: Heating
4: sodium tetrahydroborate
5: Chiralpak 1A / ethanol; hexane / Resolution of racemate
6: zinc; hydrogenchloride / water
7: ChiralCel AD
8: rhodium(III) chloride; sodium periodate
View Scheme
Multi-step reaction with 9 steps
1: N-ethyl-N,N-diisopropylamine
2: sodium hydride
3: Heating
4: sodium tetrahydroborate
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol
6: Chiralpak 1A / ethanol; hexane / Resolution of racemate
7: zinc; hydrogenchloride / water
8: ChiralCel AD
9: rhodium(III) chloride; sodium periodate
View Scheme

C13H8F2O2

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: sodium hydride
2: Heating
3: sodium tetrahydroborate
4: Chiralpak 1A / ethanol; hexane / Resolution of racemate
5: zinc; hydrogenchloride / water
6: ChiralCel AD
7: rhodium(III) chloride; sodium periodate
View Scheme
Multi-step reaction with 8 steps
1: sodium hydride
2: Heating
3: sodium tetrahydroborate
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol
5: Chiralpak 1A / ethanol; hexane / Resolution of racemate
6: zinc; hydrogenchloride / water
7: ChiralCel AD
8: rhodium(III) chloride; sodium periodate
View Scheme
951127-28-9

6-(2,5-difluorophenyl)-3-methylidene-5-nitro-3,4-dihydro-2H-pyran

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium tetrahydroborate
2: Chiralpak 1A / ethanol; hexane / Resolution of racemate
3: zinc; hydrogenchloride / water
4: ChiralCel AD
5: rhodium(III) chloride; sodium periodate
View Scheme
Multi-step reaction with 6 steps
1: sodium tetrahydroborate
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol
3: Chiralpak 1A / ethanol; hexane / Resolution of racemate
4: zinc; hydrogenchloride / water
5: ChiralCel AD
6: rhodium(III) chloride; sodium periodate
View Scheme
Multi-step reaction with 5 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 5 °C
2: hydrogenchloride; zinc / water; ethanol / 1 h / 0 °C
3: methanol / 15 h / 25 °C
4: sodium carbonate / water; acetonitrile / 2 h / 0 - 30 °C
5: sodium periodate; ruthenium(III) chloride trihydrate / water; acetonitrile; dichloromethane / 3 h / 25 °C
View Scheme

trans-5-methylene-3-nitro-2-(2,5-difluorophenyl)-tetrahydro-2H-pyran

951127-25-6

N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]carbamic acid 1,1-dimethylethyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: Chiralpak 1A / ethanol; hexane / Resolution of racemate
2: zinc; hydrogenchloride / water
3: ChiralCel AD
4: rhodium(III) chloride; sodium periodate
View Scheme
Multi-step reaction with 4 steps
1: zinc; acetic acid / ethanol / 1 h
2: dichloromethane / 20 h / 20 °C
3: Chiralpak IA / Resolution of racemate
4: sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water / 2 h / 0 °C
View Scheme
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    Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, s

  •  Shandong Mopai Biotechnology Co., LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-15965530500

    Address:shandong

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  • CPo3604-01 951127-25-6

  • Casno:

    951127-25-6

    CPo3604-01 951127-25-6

    Min.Order: 1 Metric Ton

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    1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

    KAISA GROUP INC.is the enterprise which is specialize in manfacturing and exporting avariety of Chemical in China. We have the strong economic base and comprehensive technology.We

  •  KAISA GROUP INC

    United States  |  Contact Details

    Business Type:Trading Company

    Tel:15131197030

    Address:1312 17th Street Suite 1402 Denver CO 80202

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  • N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-CarbaMic acid 1,1-diMethylethyl ester

  • Casno:

    951127-25-6

    N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-CarbaMic acid 1,1-diMethylethyl ester

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe

    SAGECHEM is a chemical R&D, manufacturing and distribution company since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and

  •  SAGECHEM LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86818502

    Address:5Fl. 501Room, Tower A, New Youth Plaza, 8 Jia Shan Road, Hangzhou, China

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  • N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-CarbaMic acid 1,1-diMethylethyl ester

  • Casno:

    951127-25-6

    N-[(2R,3S)-2-(2,5-difluorophenyl)tetrahydro-5-oxo-2H-pyran-3-yl]-CarbaMic acid 1,1-diMethylethyl ester

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Chemvon Biotechnology is one of the leading high-technology manufacturer in the field of pharmaceutical and fine chemical industry. From origins as a research group in technology service, chemvon has progressed into an integrated company with a k

    Chemvon Biotechnology Co. Ltd is a high-technology pharmaceutical and fine chemical company, which is speciallized in RD, manufacturing and sales of APIs (Active Pharmaceutical I

  •  Chemvon Biotechnology Co. Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-21-58550039;86-21-31268550-8004

    Address:Suite B-10#, 6999 Chuansha Road, Pudong District, Shanghai 201202, China

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  • Casno:

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    CPo3604-01 951127-25-6

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.0-1.0

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

    We are a Union of chemistry in China, consists of chemists，engineers, laboratories,factories in China. We organize surplus capacity of R&D and production in China for chemicals cus

  •  Bluecrystal chem-union

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-1895157

    Address:Liang Xi Qu

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  • CPo3604-01 cas no. 951127-25-6 98%

  • Casno:

    951127-25-6

    CPo3604-01 cas no. 951127-25-6 98%

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

    Established in 2007, Win-Win chemical CO., Ltd is a privately held corporation headquartered in Wenzhou Longwan Industry Distric, dedicated to the global pharmaceutical companies a

  •  Win-Win chemical Co.Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-577-64498589

    Address:No.49 YuShi West Road, Longwan District,325000

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  • Omarigliptin intermediate

  • Casno:

    951127-25-6

    Omarigliptin intermediate

    Min.Order: 0 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Why is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 37 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c

    Sinoway Industrial co., ltd. was established in 1987 in Xiamen, China, and now has been a leading group specialized in research, development, custom manufacturing and trading of ph

  •  Sinoway Industrial Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-592-583819

    Address:16/F,Huicheng Comm,Complex,No839 XiaHe Rd, Xiamen,China

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  • CPo3604-01

  • Casno:

    951127-25-6

    CPo3604-01

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    High purity, high success rate, short cycle and moderate priceAppearance:White powder solid Storage:Negative 20 degrees Celsius Package:5mg, 10mg 100mg, 1gram Application:Applied to various scientific research

    Anhui Research Peptide Biotechnology Co., Ltd. (hereinafter referred to as Specialized Peptide Biology, Hangzhou All Peptide Biology Hefei Branch) was established in 2018. It is

  •  Research Peptide Biotechnology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+87-17342063383

    Address:Room 0196, Four-storey Creative Space, EC Building, Baohe Garden Commercial Building, Baohe District.

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  • CPo3604-01

  • Casno:

    951127-25-6

    CPo3604-01

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

  •  GIHI CHEMICALS CO.,LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86217390

    Address:No.567 Dengcai Street,Sandun,Westlake District,Hangzhou310030,Zhejiang,China.

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  • CPo3604-01

  • Casno:

    951127-25-6

    CPo3604-01

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application: It is an important

    Hangzhou Yunuo Chemical Co., Ltd. is located in Hangzhou City, China We are specialized in fine chemicals and basic chemical auxiliary materials, Organic compounds, rubber

  •  HANGZHOU YUNUO CHEMICAL CO.,LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0571-83715115

    Address:hangzhou

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