14031-02-8

• 

• Basic information

  1. Product Name: 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATE
  2. Synonyms: Thiocyanicacid, 4-amino-3,5-xylyl ester (8CI); 2,6-Xylidine, 4-thiocyanato-
  3. CAS NO:14031-02-8
  4. Molecular Formula: C₉H₁₀N₂S
  5. Molecular Weight: 178.25
  6. EINECS: N/A
  7. Product Categories: N/A
  8. Mol File: 14031-02-8.mol
  9. Article Data: 9

• Chemical Properties

  1. Melting Point: N/A
  2. Boiling Point: 316.8°Cat760mmHg
  3. Flash Point: 145.4°C
  4. Appearance: /
  5. Density: 1.19g/cm³
  6. Vapor Pressure: 0.000401mmHg at 25°C
  7. Refractive Index: 1.614
  8. Storage Temp.: N/A
  9. Solubility: N/A
  10. CAS DataBase Reference: 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATE(CAS DataBase Reference)
  11. NIST Chemistry Reference: 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATE(14031-02-8)
  12. EPA Substance Registry System: 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATE(14031-02-8)

• Safety Data

  1. Hazard Codes: N/A
  2. Statements: N/A
  3. Safety Statements: N/A
  4. WGK Germany:
  5. RTECS:
  6. HazardClass: N/A
  7. PackingGroup: N/A
  8. Hazardous Substances Data: 14031-02-8(Hazardous Substances Data)

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• Article

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• 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATECAS

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• 4-AMINO-3,5-DIMETHYLPHENYL THIOCYANATE

  Cas No: 14031-02-8

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14031-02-8 Usage

Check Digit Verification of cas no

The CAS Registry Mumber 14031-02-8 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,4,0,3 and 1 respectively; the second part has 2 digits, 0 and 2 respectively.
Calculate Digit Verification of CAS Registry Number 14031-02:
(7*1)+(6*4)+(5*0)+(4*3)+(3*1)+(2*0)+(1*2)=48
48 % 10 = 8
So 14031-02-8 is a valid CAS Registry Number.

InChI:InChI=1/C9H10N2S/c1-6-3-8(12-5-10)4-7(2)9(6)11/h3-4H,11H2,1-2H3

14031-02-8SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name	(4-amino-3,5-dimethylphenyl) thiocyanate

1.2 Other means of identification

Product number	-
Other names	2,6-dimethyl-4-thiocyanatobenzenamine

1.3 Recommended use of the chemical and restrictions on use

Identified uses	For industry use only.
Uses advised against	no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number	-
Service hours	Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:14031-02-8 SDS

14031-02-8Upstream product

• 87-62-7 2,6-dimethylaniline 
• 333-20-0 potassium thioacyanate 
• 1147550-11-5 ammonium thiocyanate 
• 540-72-7 sodium thiocyanide 

14031-02-8Downstream Products

• 342044-04-6 acetic acid-(4-methanesulfonyl-2,6-dimethyl-anilide) 
• 120578-20-3 4-amino-3,5-dimethylphenyl methyl sulphide 

14031-02-8Relevant articles and documents

Efficient and novel method for thiocyanation of aromatic and heteroaromatic compounds using bromodimethylsulfonium bromide and ammonium thiocyanate

Bhalerao, Dinesh S.,Akamanchi, Krishnacharya G.

, p. 2952 - 2956 (2007)

Various aromatic and heteroaromatic compounds have been efficiently thiocyanated by using a novel combination of bromodimethylsulfonium bromide (BDMS) and ammonium thiocyanate. Georg Thieme Verlag Stuttgart.

Transition-metal-free regioselective thiocyanation of phenols, anilines and heterocycles

Mete, Trimbak B.,Khopade, Tushar M.,Bhat, Ramakrishna G.

, p. 415 - 418 (2017)

An expedient direct and regioselective thiocyanation of phenols, anilines and heterocycles is described. Transformation is realized via the direct C[sbnd]H functionalization under transition metal free conditions at ambient temperature in excellent yields. Method proved to be monoselective and variety of functional groups tolerated the reaction conditions. The practicality of the protocol is demonstrated in gram scale synthesis of a precursor of PPAR δ agonist in excellent yield.

Rapid and efficient thiocyanation of phenols, indoles, and anilines in 1,1,1,3,3,3-hexafluoro-2-propanol under ultrasound irradiation

Wang, Zhonghao,Wang, Liang,Chen, Qun,He, Ming-yang

supporting information, p. 76 - 84 (2017/12/28)

An efficient ultrasound-promoted thiocyanation of phenols, indoles, and anilines in the presence of N-chlorosuccinimide and NH4SCN using 1,1,1,3,3,3-hexafluoro-2-propanol as the solvent has been developed. The major features of the present protocol include the mild reaction conditions, short reaction times, good to excellent yields, and broad substrate scope. Moreover, scale-up synthesis can be achieved and the solvent can be easily recovered and reused.

Catalytic Thiourea Promoted Electrophilic Thiocyanation of Indoles and Aromatic Amines with NCS/NH4SCN

Wang, Cancan,Wang, Zhonghao,Wang, Liang,Chen, Qun,He, Mingyang

supporting information, p. 1081 - 1085 (2016/11/25)

A simple and efficient protocol for the electrophilic thiocyanation of indoles and aromatic amines with thiourea/NCS/NH4SCN system has been developed. The major features of the present procedure are the mild conditions, good yields, short reaction times, and the use of inexpensive and readily available organocatalyst. Moreover, N-chlorosuccinimide (NCS) was found to be indispensable, and thiourea could greatly promote the reaction.

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