159878-02-1

• 

• Basic information

  1. Product Name: Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate
  2. Synonyms: Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate;(2S,3R)-3-N-CBZ-AMINO-1-CHLORO-4-(PHENYLTHIO)BUTAN-2-OL;N-[(1R,2S)-3-Chloro-2-hydroxy-1-[(phenylthio)Methyl]propyl]carbaMic Acid PhenylMethyl Ester;benzyl ((2R,3S)-4-chloro-3-hydroxy-1-(phenylthio)butan-2-yl)carbaMate;CarbaMic acid,N-[(1R,2S)-3-chloro-2-hydroxy-1-[(phenylthio)Methyl]propyl]-, phenylMethylester;Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate-5;(2S,3R)-3-CARBOBENZYLOXYAMINO-1-CHLORO-4-PHENYLTHIO-BUTAN-2-OL;(2S,3R)-N-Cbz-3-amino-1-chloro-4-(phenylthio)butan-2-ol
  3. CAS NO:159878-02-1
  4. Molecular Formula: C₁₈H₂₀ClNO₃S
  5. Molecular Weight: 365.87
  6. EINECS: N/A
  7. Product Categories: API intermediates;Chiral Reagents;Miscellaneous Reagents;Sulfur & Selenium Compounds;Aromatics
  8. Mol File: 159878-02-1.mol
  9. Article Data: 9

• Chemical Properties

  1. Melting Point: 114-116°C
  2. Boiling Point: 559.88 °C at 760 mmHg
  3. Flash Point: 292.405 °C
  4. Appearance: White solid
  5. Density: 1.292 g/cm³
  6. Vapor Pressure: 0mmHg at 25°C
  7. Refractive Index: 1.617
  8. Storage Temp.: Refrigerator
  9. Solubility: Chloroform, Methanol
  10. CAS DataBase Reference: Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate(CAS DataBase Reference)
  11. NIST Chemistry Reference: Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate(159878-02-1)
  12. EPA Substance Registry System: Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate(159878-02-1)

• Safety Data

  1. Hazard Codes: N/A
  2. Statements: N/A
  3. Safety Statements: N/A
  4. WGK Germany:
  5. RTECS:
  6. HazardClass: N/A
  7. PackingGroup: N/A
  8. Hazardous Substances Data: 159878-02-1(Hazardous Substances Data)

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• SDS
• Upstream product
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159878-02-1 Suppliers

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• (2S,3R)-N-Benzyloxycarbonyl-3-amino-1-chloro-4-(phenylthio)-2-butanol

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• Benzyl (1R,2S)-3-chloro-2-hydroxy-1-(phenylthiomethyl)propylcarbamate CAS:159878-02-1

  Cas No: 159878-02-1

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• Carbamic acid,N-[(1R,2S)-3-chloro-2-hydroxy-1-[(phenylthio)methyl]propyl]-, phenylmethylester

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• Xiamen Hisunny Chemical Co.,Ltd
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• Carbamic acid,N-[(1R,2S)-3-chloro-2-hydroxy-1-[(phenylthio)methyl]propyl]-, phenylmethylester

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159878-02-1 Usage

Chemical Properties

White Solid

Uses

(2S,3R)-3-Carbobenzyloxyamino-1-chloro-4-phenylthio-butan-2-ol (cas# 159878-02-1) is a compound useful in organic synthesis.

Check Digit Verification of cas no

The CAS Registry Mumber 159878-02-1 includes 9 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 6 digits, 1,5,9,8,7 and 8 respectively; the second part has 2 digits, 0 and 2 respectively.
Calculate Digit Verification of CAS Registry Number 159878-02:
(8*1)+(7*5)+(6*9)+(5*8)+(4*7)+(3*8)+(2*0)+(1*2)=191
191 % 10 = 1
So 159878-02-1 is a valid CAS Registry Number.

InChI:InChI=1/C18H20ClNO3S/c19-11-17(21)16(13-24-15-9-5-2-6-10-15)20-18(22)23-12-14-7-3-1-4-8-14/h1-10,16-17,21H,11-13H2,(H,20,22)/t16-,17+/m0/s1

159878-02-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name	(2S,3R)-3-Carbobenzyloxyamino-1-chloro-4-phenylthio-butan-2-ol

1.2 Other means of identification

Product number	-
Other names	benzyl N-[(2R,3S)-4-chloro-3-hydroxy-1-phenylsulfanylbutan-2-yl]carbamate

1.3 Recommended use of the chemical and restrictions on use

Identified uses	For industry use only.
Uses advised against	no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number	-
Service hours	Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:159878-02-1 SDS

159878-02-1Upstream product

• 197302-33-3 benzyl [(2R)-1-[methoxy(methyl)amino]-1-oxo-3-(phenylsulfanyl)-2-propanyl]carbamate 
• 159878-01-0 (R)-(1-phenylthiomethyl-3-chloro-2-oxopropyl)carbamic acid benzyl ester 
• 82611-65-2 N-benzyloxycarbonyl-S-phenyl-L-cysteine 
• 555-31-7 aluminum isopropoxide 
• 246252-56-2 (4S,1'S)-4-[1'-(N-benzyloxycarbonyl)amino-2'-hydroxyethyl]-2,2-dimethyl-1,3-dioxolane 
• 115887-84-8 (2R,3S)-2-(N-benzyloxycarbonyl)amino-3-hydroxy-4-butanolide 

159878-02-1Downstream Products

• 163462-16-6 benzyl [(1R)-1-[(2S)-2-oxiranyl]-2-(phenylsulfanyl)ethyl]carbamate 

159878-02-1Relevant articles and documents

Merging lithium carbenoid homologation and enzymatic reduction: A combinative approach to the HIV-protease inhibitor Nelfinavir

Castoldi, Laura,Ielo, Laura,Hoyos, Pilar,Hernáiz, María J.,De Luca, Laura,Alcántara, Andrés R.,Holzer, Wolfgang,Pace, Vittorio

, p. 2211 - 2217 (2018/03/28)

An effective stereocontrolled synthesis of the HIV protease inhibitor Nelfinavir is reported. Two transformations were identified crucial for achieving success: the formation of a densely functionalized α-chloroketone via the homologation of a Weinreb ami

Development of a continuous process for the industrial generation of diazomethane

Proctor, Lee D.,Warr, Antony J.

, p. 884 - 892 (2013/09/06)

The development of a safe process for the industrial generation of diazomethane is described. Diazomethane is produced and consumed in a continuous process capable of generating between 50 and 60 tonnes per year whilst the maximum inventory is maintained

Process for reducing α-amino ketones

-

, (2008/06/13)

The present invention has its objects to provide a method for reducing α-aminoketone derivatives under mild conditions with high stereoselectivity. This invention is a method for reducing α-aminoketone which comprises reacting an a-aminoketone derivative of general formula (1) with a compound prepared from an organoaluminum compound of general formula (4), a sulfonic acid derivative of general formula (5), and an alcohol compound of general formula (6) to give an α-aminoalcohol derivative of general formula (7)

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