17714-57-7Relevant articles and documents
Elliott et al.
, p. 167,168 (1967)
Preparation method of indanone compound
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Paragraph 0035-0044; 0052-0081, (2021/08/07)
The invention provides a preparation method of a hydrindone compound, and belongs to the technical field of compound synthesis. The method comprises the following steps: under the action of a nickel catalyst, a ligand, bis(pinacolato)diboron, alkali and water, reacting o-bromophenyl cyclobutanone of a formula 1 structure in a solvent at 70-90 DEG C for 12-24 hours, and separating and purifying a product after the reaction is finished to obtain the indanone compound of the formula I structure. The method is simple, raw materials are easy to obtain, experimental operation is simple and convenient, and the yield of the prepared product is moderate.
Microwave-assisted one-pot synthesis of 1-indanones from arenes and α,β-unsaturated acyl chlorides
Yin, Wei,Ma, Yuan,Xu, Jiaxi,Zhao, Yufen
, p. 4312 - 4315 (2007/10/03)
A series of 1-indanones were synthesized in good yields via tandem Friedel-Crafts acylation and Nazarov cyclization of arenes and α,β-unsaturated acyl chlorides in the presence of aluminum chloride under microwave irradiation.
