19485-63-3

• 

• Basic information

  1. Product Name: 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol
  2. Synonyms: 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol;Lophocerine
  3. CAS NO:19485-63-3
  4. Molecular Formula: C15H23NO2
  5. Molecular Weight: 0
  6. EINECS: N/A
  7. Product Categories: N/A
  8. Mol File: 19485-63-3.mol
  9. Article Data: 2

• Chemical Properties

  1. Melting Point: N/A
  2. Boiling Point: 358.3°C at 760 mmHg
  3. Flash Point: 170.5°C
  4. Appearance: /
  5. Density: 1.035g/cm³
  6. Vapor Pressure: 1.25E-05mmHg at 25°C
  7. Refractive Index: 1.525
  8. Storage Temp.: N/A
  9. Solubility: N/A
  10. CAS DataBase Reference: 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol(CAS DataBase Reference)
  11. NIST Chemistry Reference: 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol(19485-63-3)
  12. EPA Substance Registry System: 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol(19485-63-3)

• Safety Data

  1. Hazard Codes: N/A
  2. Statements: N/A
  3. Safety Statements: N/A
  4. WGK Germany:
  5. RTECS:
  6. HazardClass: N/A
  7. PackingGroup: N/A
  8. Hazardous Substances Data: 19485-63-3(Hazardous Substances Data)

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• SDS
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• Downstream Products
• Article

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• 1,2,3,4-Tetrahydro-6-methoxy-2-methyl-1-(2-methylpropyl)isoquinolin-7-ol

  Cas No: 19485-63-3

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19485-63-3 Usage

Description

This alkaloid belongs to the isoquinoline group and is one of the cactus bases being found in Lophocereus schottii. It is a colourless oil giving a crystalline picrate and a styphnate with m.p. 191.5-193°C and 171-2°C respectively. The structure has been established as 1:2:3:4-tetrahydro-7-hydroxy-l-isobutyl-6- methoxy-2-methylisoquinoline. It yields a methyl ether, forming a picrate, m.p. 180-2°C and a styphnate, m.p. 210-2°C. The corresponding ethyl ether also gives a picrate and styphnate with m.p. ISO-3°C and 182-3°C respectively.

Synthesis Reference(s)

The Journal of Organic Chemistry, 24, p. 1106, 1959 DOI: 10.1021/jo01090a018

References

Bobbitt, Chou., J. Org. Chem., 24, 1106 (1959)

Check Digit Verification of cas no

The CAS Registry Mumber 19485-63-3 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,9,4,8 and 5 respectively; the second part has 2 digits, 6 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 19485-63:
(7*1)+(6*9)+(5*4)+(4*8)+(3*5)+(2*6)+(1*3)=143
143 % 10 = 3
So 19485-63-3 is a valid CAS Registry Number.

InChI:InChI=1/C15H23NO2/c1-10(2)7-13-12-9-14(17)15(18-4)8-11(12)5-6-16(13)3/h8-10,13,17H,5-7H2,1-4H3

19485-63-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name	6-methoxy-2-methyl-1-(2-methylpropyl)-3,4-dihydro-1H-isoquinolin-7-ol

1.2 Other means of identification

Product number	-
Other names	7-Hydroxy-6-methoxy-2-methyl-1-isobutyl-1,2,3,4-tetrahydro-isochinolin

1.3 Recommended use of the chemical and restrictions on use

Identified uses	For industry use only.
Uses advised against	no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number	-
Service hours	Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:19485-63-3 SDS

19485-63-3Upstream product

• 95160-06-8 7-benzyloxy-1-isobutyl-6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline 
• 122765-87-1 7-benzyloxy-1-isobutyl-6-methoxy-2-methyl-3,4-dihydro-isoquinolinium; iodide 
• 97254-91-6 7-benzyloxy-1-isobutyl-6-methoxy-3,4-dihydro-isoquinoline 
• 22231-61-4 2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine 
• 106412-31-1 7-benzyloxy-6-methoxy-2-methoxycarbonyl-1-(2-methyl-1-propen-1-yl)-1,2,3,4-tetrahydroisoquinoline 
• 106412-28-6 4-<5-benzyloxy-4-methoxy-2-(2-nitroethyl)phenyl>-2-methyl-3-buten-2-ol 
• 106412-26-4 4-<5-benzyloxy-4-methoxy-2-(2-nitrovinyl)phenyl>-2-methyl-3-buten-2-ol 
• 106412-30-0 1-(2-methyl-1-propen-1-yl)-6,7-6-methoxy,7-enzyloxy-1,2,3,4-tetrahydroisoquinoline 
• 106412-24-2 4-benzyloxy-2-(3-hydroxy-3-methyl-1-butenyl)-5-methoxybenzaldehyde 
• 40705-22-4 4-benzyloxy-6-bromo-3-methoxybenzaldehyde 
• 115-18-4 2-methyl-3-buten-2-ol 
• 106412-32-2 7-benzyloxy-6-methoxy-2-methyl-1-(2-methyl-1-propen-1-yl)-1,2,3,4-tetrahydroisoquinoline 
• 95290-23-6 N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-3-methylbutyramide 
• 63909-38-6 3-methoxy-4-benzyloxy-ω-nitrostyrolene 

19485-63-3Downstream Products

19485-63-3Relevant articles and documents

A novel reductive amino-cyclization method and its application for the total syntheses of (±)-aurantio-clavine and (±)-lophocerine

Somei, Masanori,Yamada, Fumio

, p. 943 - 950 (2008/09/19)

A novel reductive amino-cyclization method for the synthesis of azacycloalkanes is developed. Its versatility is proved by the total syntheses of (±)-aurantioclavine (1), an ergot alkaloid, and (±)-lophocerine (2), a cactus alkaloid, as examples of azepan

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