103725-76-4Relevant articles and documents
Synthesis of Pro-Pro-Ile, a corticoliberin fragment, labeled with tritium in proline unit
Shevchenko,Nagaev, I. Yu.,Andreeva,Myasoedov
experimental part, p. 325 - 329 (2011/01/10)
Boc-δ3Pro-Pro-Ile-OBzl and Boc-Pro-δ3Pro- Ile-OBzl were synthesized. Tritium-labeled Pro-Pro-Ile was prepared by their hydrogenation in a tritium atmosphere in the presence of a catalyst. In the reduction of Boc-δ3Pro-Pro-Ile-OBzl and Boc-Pro- δ3Pro-Ile-OBzl, elimination of the Bzl protective group occurs faster than hydrogenation of the 3,4-dehydroproline residue (benzene and dioxane were used as solvents). The resulting Boc-δ3Pro-Pro-Ile-OH and Boc-Pro-δ3Pro-Ile-OH are poorly soluble in aprotic solvents, which accounts for the low yield of the desired tritium-labeled peptides. Pleiades Publishing, Inc., 2010.
Structure of Halo-toxin Procedured by Phytopathogenic Bacterium, Pseudomonas syringae pv. mori
Kajimoto, Tetsuya,Yokomizo, Kazumi,Yahiro, Kiyoshi,Umeda, Toshiko,Shoji, Shozo,et al.
, p. 679 - 680 (2007/10/02)
Halo-toxin was isolated from the incubated medium of Pseudomonas syringae pv. mori which causes halo bright disease against the leaves of mulberry trees.The structure of this compound was revealed to be Pro-Phe-Pro-Gly-Pro-Ile by spectroscopic means and a