104091-35-2Relevant articles and documents
Anomalously coupled nucleosides, I.- Tributylammonium phosphates in chloroform for direct coupling of 2-deoxy-D-ribose with N6-substituted adenines
Andersen, Jesper,Pedersen, Erik B.
, p. 1837 - 1846 (2007/10/02)
Phosphorus pentoxide reacts with water and tributylamine in chloroform to give a homogeneous solution of tributylammonium phosphate, pyrophosphate, and trimetaphosphate. 3-(9-Adenyl)-2,3-dideoxy-D-threo-pentopyranoses 3 precipitate on treatment of 2-deoxy-D-ribose (2) with N6-substituted adenines 1 in this solution at 40 deg C after 7 days.