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2206-26-0

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2206-26-0 Usage

Chemical Properties

colourless liquid

Uses

Different sources of media describe the Uses of 2206-26-0 differently. You can refer to the following data:
1. Acetonitrile-d3 is used as a polar aprotic solvent in organic synthesis.
2. Isotope labeled Acetonitrile is used as a polar aprotic solvent in organic synthesis. Acetonitrile-d3 is used as IR and NMR solvent. Probe for zeolite acidity. Cartridge eluent in HPLC- SPE (solid-phase extraction)-NMR technique.
3. Acetonitrile-d3 may be used as:IR and NMR solvent.Probe for zeolite acidity.Cartridge eluent in HPLC– SPE (solid-phase extraction)–NMR technique.

General Description

Acetonitrile-d3 (Trideuteroacetonitrile, CD3CN) is a deuterated NMR (Nuclear Magnetic Resonance) solvent. Molecular rotational friction coefficient and magnetic relaxation times (T1) for 14N and 2D of CD3CN have been determined. It participates as solvent during the synthesis of 2-phenylindole. It serves as solvent for 1H NMR (Proton Nuclear Magnetic Resonance) and 13C NMR (Carbon-13 Nuclear Magnetic Resonance) spectral studies.

Check Digit Verification of cas no

The CAS Registry Mumber 2206-26-0 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 2,2,0 and 6 respectively; the second part has 2 digits, 2 and 6 respectively.
Calculate Digit Verification of CAS Registry Number 2206-26:
(6*2)+(5*2)+(4*0)+(3*6)+(2*2)+(1*6)=50
50 % 10 = 0
So 2206-26-0 is a valid CAS Registry Number.
InChI:InChI=1/C2H3N/c1-2-3/h1H3/i1D3

2206-26-0 Well-known Company Product Price

  • Brand
  • (Code)Product description
  • CAS number
  • Packaging
  • Price
  • Detail
  • Alfa Aesar

  • (42266)  Acetonitrile-d3, 100% (Isotopic)   

  • 2206-26-0

  • 2each

  • 492.0CNY

  • Detail
  • Alfa Aesar

  • (42266)  Acetonitrile-d3, 100% (Isotopic)   

  • 2206-26-0

  • 10each

  • 2464.0CNY

  • Detail
  • Alfa Aesar

  • (42264)  Acetonitrile-d3, 99.8% (Isotopic)   

  • 2206-26-0

  • 2g

  • 177.0CNY

  • Detail
  • Alfa Aesar

  • (42264)  Acetonitrile-d3, 99.8% (Isotopic)   

  • 2206-26-0

  • 10g

  • 640.0CNY

  • Detail
  • Alfa Aesar

  • (42264)  Acetonitrile-d3, 99.8% (Isotopic)   

  • 2206-26-0

  • 50g

  • 3042.0CNY

  • Detail
  • Aldrich

  • (569550)  Acetonitrile-d3  ≥99.8 atom % D, anhydrous

  • 2206-26-0

  • 569550-10X1ML

  • 6,499.35CNY

  • Detail
  • Aldrich

  • (233323)  Acetonitrile-d3  "100%", 99.96 atom % D

  • 2206-26-0

  • 233323-10X0.5ML

  • 1,811.16CNY

  • Detail
  • Aldrich

  • (233323)  Acetonitrile-d3  "100%", 99.96 atom % D

  • 2206-26-0

  • 233323-5G

  • 1,574.82CNY

  • Detail
  • Aldrich

  • (233323)  Acetonitrile-d3  "100%", 99.96 atom % D

  • 2206-26-0

  • 233323-10X0.75ML

  • 2,164.50CNY

  • Detail
  • Aldrich

  • (233323)  Acetonitrile-d3  "100%", 99.96 atom % D

  • 2206-26-0

  • 233323-25G

  • 7,055.10CNY

  • Detail
  • Aldrich

  • (151807)  Acetonitrile-d3  ≥99.8 atom % D

  • 2206-26-0

  • 151807-5G

  • 469.17CNY

  • Detail
  • Aldrich

  • (151807)  Acetonitrile-d3  ≥99.8 atom % D

  • 2206-26-0

  • 151807-10X0.6ML

  • 570.96CNY

  • Detail

2206-26-0Relevant articles and documents

Reaction of 3-Chloro-3-methyldiazirines with Hydrogen Atoms

Burkholder, C. D.,Jones, W. E.,Wasson, J. S.,Liu, M. T. H.

, p. 2847 - 2848 (1980)

-

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Leitch

, p. 345 (1957)

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Organocatalytic Deuteration Induced by the Dynamic Covalent Interaction of Imidazolium Cations with Ketones

Ananikov, Valentine P.,Galkin, Konstantin I.,Gordeev, Evgeniy G.

supporting information, p. 1368 - 1378 (2021/01/18)

In this article, we suggest a new organocatalytic approach based on the dynamic covalent interaction of imidazolium cations with ketones. A reaction of N-alkyl imidazolium salts with acetone-d6 in the presence of oxygenated bases generates a dynamic organocatalytic system with a mixture of protonated carbene/ketone adducts acting as H/D exchange catalysts. The developed methodology of the pH-dependent deuteration showed high selectivity of labeling and good chiral functional group tolerance. Here we report a unique methodology for efficient metal-free deuteration, which enables labeling of various types of α-acidic compounds without trace metal contamination. (Figure presented.).

Ruthenium-catalyzed selective α-deuteration of aliphatic nitriles using D2O

Krishnakumar, Varadhan,Gunanathan, Chidambaram

supporting information, p. 8705 - 8708 (2018/08/07)

Selective catalytic α-deuteration of aliphatic nitriles using deuterium oxide as a deuterium source is reported. A PNP-ruthenium pincer complex catalyzed the α-deuteration of aliphatic nitriles including acetonitrile. Efficient deuteration occurred with a low catalyst load (0.2 to 0.5 mol%) and under mild conditions. A [2+2] cycloadduct formation from nitrile functionality and a deprotonated catalytic intermediate, followed by an imine-enamine tautomerization and a H/D exchange between the enamine intermediate and deuterium oxide leading to the selective deuteration at the α-position of the nitrile, is proposed as a plausible reaction mechanism.

(2+2)-Cycloreversionsprodukte aus 2-(Methylazo)propen?

Remmler, Matthias,Ondruschka, Bernd,Ziegler, Ulrich,Zimmermann, Gerhard

, p. 396 - 397 (2007/10/02)

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