56776-45-5

Basic information

• Product Name: 2,3'-Dimethylbenzanilide
• Synonyms: 2,3'-Dimethylbenzanilide;2-Methyl-N-(3-methylphenyl)benzamide;2-Methyl-N-(M-tolyl)benzaMide
• CAS NO: 56776-45-5
• Molecular Formula: C₁₅H₁₅NO
• Molecular Weight: 225.2857
• Mol File: 56776-45-5.mol
• Article Data: 2

Chemical Properties

• Melting Point: 144℃
• Boiling Point: 292.9 °C at 760 mmHg
• Flash Point: 174.5 °C
• Appearance: /
• Density: 1.21
• Vapor Pressure: 0.00179mmHg at 25°C
• Refractive Index: 1.619
• CAS DataBase Reference: 2,3'-Dimethylbenzanilide(CAS DataBase Reference)
• NIST Chemistry Reference: 2,3'-Dimethylbenzanilide(56776-45-5)
• EPA Substance Registry System: 2,3'-Dimethylbenzanilide(56776-45-5)

Safety Data

• Hazardous Substances Data: 56776-45-5(Hazardous Substances Data)

Usage

General Description

2,3'-Dimethylbenzanilide is a chemical compound with the formula C15H15NO. It is a white crystalline solid that is commonly used as an intermediate in the production of various dyes and pigments. 2,3'-Dimethylbenzanilide is known for its role as a key ingredient in the synthesis of azo dyes. It is also used as a fragrance and flavoring agent in the cosmetic and food industries. Additionally, 2,3'-Dimethylbenzanilide has been studied for its potential pharmaceutical applications, particularly its anti-inflammatory and analgesic properties. However, it is important to handle this compound with caution as it may pose risks to human health and the environment if not properly managed.

InChI:InChI=1/C15H15NO/c1-11-6-5-8-13(10-11)16-15(17)14-9-4-3-7-12(14)2/h3-10H,1-2H3,(H,16,17)

Upstream product

• 933-88-0 ortho-toluoyl chloride 
• 108-44-1 1-amino-3-methylbenzene 
• 118-90-1 ortho-methylbenzoic acid 
• 84053-11-2 2-amino-3-(4-mercaptophenyl)propanoic acid 

Downstream Products

• 317374-07-5 2-bromo-5-(2-methylbenzoylamino)toluene 
• 928151-35-3 2-chloro-2'-methyl-4'-(2-methylbenzoylamino)-acetophenone 
• 928151-36-4 2-chloro-4'-methyl-2'-(2-methylbenzoylamino)aceto-phenone 
• 928151-34-2 2-methyl-4-(2-methylbenzoylamino)acetophenone 

Relevant articles and documents

Method for synthesizing amide compound through photocatalysis in water phase

The invention discloses a method for synthesizing an amide compound through photocatalysis in a water phase. The method comprises the following steps: putting catalysis amounts of a free radical initiator, an amine derivative, a carboxylic acid derivative, a phase transfer catalyst, an inorganic base and water into a reaction container, carrying out a reaction in a photocatalysis reaction instrument at certain power under a room temperature condition, after a certain time, carrying out extraction by using a small amount of ethyl acetate, and carrying out recrystallization, so as to obtain theamide compound, wherein the free radical initiator is eosin, methyl orange, sodium persulfate, ammonium persulfate or potassium peroxodisulfate, the phase transfer catalyst is tetrabutylammonium bromide, and the power of the photocatalytic reaction instrument is 5W. By adopting the method disclosed by the invention, toxic thionyl chloride or phosphorus oxychloride is not needed for a chlorinationreaction, water is adopted as a solvent, a novel photocatalysis method is used, and the amide compound with a high yield can be prepared through a room-temperature reaction for 2-5 hours with an incandescent light bulb of 5W, and in addition, the method is simple in aftertreatment, and low in cost and is an ideal green synthesis method of amide compounds.