6631-69-2

Basic information

• Product Name: 4-(2-iodoethyl)phenol
• CAS NO: 6631-69-2
• Molecular Formula: C₈H₉IO
• Molecular Weight: 248.0609
• Mol File: 6631-69-2.mol
• Article Data: 11

Chemical Properties

• Boiling Point: 306.1°C at 760 mmHg
• Flash Point: 138.9°C
• Density: 1.778g/cm³
• Vapor Pressure: 0.000437mmHg at 25°C
• Refractive Index: 1.646
• CAS DataBase Reference: 4-(2-iodoethyl)phenol(CAS DataBase Reference)
• NIST Chemistry Reference: 4-(2-iodoethyl)phenol(6631-69-2)
• EPA Substance Registry System: 4-(2-iodoethyl)phenol(6631-69-2)

Safety Data

• Hazardous Substances Data: 6631-69-2(Hazardous Substances Data)

Upstream product

• 702-23-8 2-(4-Methoxyphenyl)ethanol 
• 156-38-7 4-hydroxyphenylacetate 
• 501123-58-6 di[2-(4-hydroxyphenyl)]ethyl ether 
• 501-94-0 p-hydroxyphenethyl alcohol 

Downstream Products

• 539-15-1 N,N-dimethyltyramine 
• 170962-05-7 4-(2-(diethylamino)ethyl)phenol 
• 74447-34-0 1-azido-2-(4-hydroxyphenyl)ethane 
• 100968-72-7 4-amino-2-hydroxy-benzoic acid-[4-(2-iodo-ethyl)-phenyl ester] 
• 6632-04-8 4-nitro-benzoic acid-[4-(2-iodo-ethyl)-phenyl ester] 
• 501-94-0 p-hydroxyphenethyl alcohol 
• 6631-80-7 N-(4-hydroxyphenethyl)morpholine 
• 82966-19-6 1-<(4-Hydroxy-phenyl)-ethyl>-piperidin 

Relevant articles and documents

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Indium(III)-catalyzed reductive bromination and iodination of carboxylic acids to alkyl bromides and iodides: Scope, mechanism, and one-pot transformation to alkyl halides and amine derivatives

Highly effective indium(III)-catalyzed reductive bromination or iodination of a variety of carboxylic acids with 1,1,3,3-tetramethyldisiloxane (TMDS) and a source of bromine or iodine is described. This functional group interconversion has high tolerance for several functional groups, such as halogens, a hydroxy group, a nitro group, an olefin part, and a sulfide moiety. This indium catalytic system is also applicable to the reductive iodination of aldehyded, acyl chlorides, and esters. Furthermore, this reducing system can be applied to the one-pot synthesis of alkyl halides and amine derivatives via the addition of nucleophiles. Insight into the reaction mechanism was gained via the time course of 1H and 13C NMR monitoring experiments and the corresponding stepwise reactions.