67684-01-9Relevant articles and documents
SYNTHESE D'IMINES CYCLIQUES NON-STABILISEES PAR REACTIONS GAZ-SOLIDE SOUS VIDE ET THERMOLYSE-ECLAIR (1,2).
Guillemin, Jean-Claude,Denis, Jean-Marc,Lasne, Marie-Claire,Ripoll, Jean-Louis
, p. 4447 - 4456 (2007/10/02)
Unstabilized cyclic imines 1-4 were synthetized in gram-scale by vacuum dehydrochlorination of N-chlorocycloamines.Azirine 5 was prepared by flash vacuum thermolysis of the corresponding vinylazide 19.All the new compounds were characterized at low temperature by 1H, 13C NMR and IR spectroscopy.