923023-81-8Relevant articles and documents
Synthesis and structure of bis(2-phenylethyl) phosphine selenide
Sukhov,Gusarova,Ivanova,Bogdanova,Kazheva,Aleksandrov,D'Yachenko,Sinegovskaya,Malysheva,Trofimov
, p. 1066 - 1071 (2005)
Bis(2-phenylethyl)phosphine selenide was obtained with 86% yield from bis(2-phenylethyl)phosphine and selenium. XRD, IR, UV, and multinuclear NMR spectroscopic studies revealed that the phosphorus atom in the bis(2-phenylethyl)phosphine selenide molecule
Green synthesis of tertiary alkylselanylphosphine chalcogenides via catalyst-and solvent-free addition of secondary phosphine chalcogenides to vinyl selenides
Gusarova,Chernysheva,Yas'Ko,Trofimov
, p. 526 - 534 (2015/10/19)
Secondary phosphine sulfides and phosphine selenides react with vinyl selenides under mild conditions (80-82°C, without catalyst and solvent) to form regioselectively functionalized anti-Markovnikov adducts in high yield.
Reaction of vinyl selenides with secondary phosphines and elemental selenium: One-pot selective synthesis of a new family of diselenophosphinic se-esters
Artem'Ev, Alexander V.,Chernysheva, Nataliya A.,Gusarova, Nina K.,Yas'Ko, Svetlana V.,Liao, Jian-Hong,Liu,Albanov, Alexander I.,Trofimov, Boris A.
, p. 135 - 139 (2014/06/09)
Alkyl vinyl selenides react with diverse secondary phosphines and elemental selenium in a 1.1:1:2 molar ratio (120-124°C, 20-40 min, 1,4-dioxane) to afford selectively earlier unknown diselenophosphinic Se-esters, R 2P(Se)SeCH(Me)SeR, in 82-99%