Welcome to LookChem.com Sign In|Join Free
  • or
Henan Tianfu Chemical Co., Ltd.122-40-7//file1.lookchem.com/cas/reactions/2021/05/31/511292.png
qq

Communicate with Supplier:

Mr. Anson
Mr. Anson: What can I do for you?

122-40-7 CAS NO.122-40-7

Min.Order Quantity:
100 Gram
Purity:
99%
Port:
China main port
Payment Terms:
L/C,T/T,MoneyGram

Add to Inquiry Cart

Product Details

Keywords

  • Heptanal,2-(phenylmethylene)-
  • FEMA 2061
  • A-PENTYLCINNAMALDEHYDE

Quick Details

  • ProName: 122-40-7
  • CasNo: 122-40-7
  • Molecular Formula: C14H18O
  • Appearance: White powder
  • Application: Organic Chemicals
  • DeliveryTime: 2 weeks
  • PackAge: in alumium foil bag
  • Port: China main port
  • ProductionCapacity: 10 Kilogram/Week
  • Purity: 99%
  • Storage: Room temperature
  • Transportation: AS PER MSDS
  • LimitNum: 100 Gram
  • Heavy metal: N/A
  • Grade: Industrial Grade,Pharma Grade
  • Transportation: N/A

Superiority

heptanal,2-(phenylmethylene)-

fema 2061;jasminal;a-pentylcinnamaldehyde;aca;a-amyl cinnamic aldehyde;alpha-pentylcinnamaldehyde;alpha-n-amylcinnamaldehyde;alpha-n-amyl cinnamic aldehyde

the properties of methyl permethaldehyde
boiling point 287-290 ° c (lit.)
density 0.97 g / ml at 25 ° c (lit.)
fema 2061
refractive index n20 / d 1.557 (lit.)
flash point> 230 ° f
storage conditions 2-8 ° c
cas database 122-40-7 (cas database reference)
nist chemical information heptanal, 2- (phenylmethylene) - (122-40-7)
epa chemical information heptanal, 2- (phenylmethylene) - (122-40-7)
production and synthesis of methyl permethaldehyde
the content analysis was determined by the method in the ester assay (ot-18). sample volume of 1.3g, the calculation of the equivalent factor (e) take 109.1. or as determined by the non-polar column method of gt-10-4.
the content analysis method accurately weighed about 1.5 g of the sample and then determined by the method of aldehyde detection (ot-7). the equivalent factor in the calculation (e = 101.2.
method two was determined by gas chromatography (gc-10-4) using a polar column.
toxicity gras (fema).
toxicity ld503730mg / kg (rat, oral).
the use of limited fema (mg / kg): soft drinks 1.3; cold 1.5; candy 4.0; baked goods 4.5; pudding 0.03 ~ 0.05;
use limited fema (mg / kg): soft drink 3.1; cold drink 4.2; candy 13; baked food 13.
moderate limit (fda $ 172.515, 2000).

Details

chemical properties yellow oily liquid. soluble in acetone.
use gb 2760 a 1996 provisions for the use of food spices. mainly for the preparation of jasmine, apples, apricots, peaches, strawberries, walnuts and spices and other fragrances.
use gb 2760--1996 provides for the use of food spices. mainly used for the preparation of vanilla and chocolate flavor.
use is a widely used important spices, and phenylethanol with comparable jasmine ketone for a variety of floral formula, especially jasmine, lily of the valley, lilac and so on. in the soap with the essence of the general dosage of 2% -10%. also can be used as edible spices, trace for apples, apricots, peaches, strawberries, walnuts and aroma and other flavor.
uses are widely used in various types of fragrance, the deployment of jasmine, lily of the valley, lilac, etc., in the soap with the usual amount of 2 to 10%, in special circumstances up to 30 to 35%. instead of or part of the replacement of methyl hexyl cinnamaldehyde for low-grade soap with detergent fragrance can be more sudden floral.
use α-amyl cinnamaldehyde is a permissible use of our food spices, can be used to prepare apples, apricots, peaches, strawberries and other food flavor. consumption in the normal production needs, generally in the chewing gum 15mg / kg; baking food 4.5mg / kg; candy 4.0mg / kg; cold drink 1.5mg / kg; soft drinks 1.3mg / kg.
use as an important ingredient in jasmine flavor, but also for lilac, hyacinth and other spices and soap spices
production method in alkaline ethanol solution, heptaldehyde and benzaldehyde are condensed into methyl permethylethylaldehyde: 8kg of 85% koh solution is dissolved in 50kg of 95% ethanol. 100 kg of benzaldehyde, 15 kg of potassium hydroxide solution and 50 kg of ethanol were added to the reaction kettle. the mixture was heated and maintained at 25 to 28 ° c while 43 kg of heptaldehyde and 43 kg of potassium hydroxide were added dropwise. after 6 h, the mixture was stirred for 2 hours, after washing the ethanol after the refractive index in the n d20 1.549 above the end of the reaction. the reaction is neutralized and the ethanol is recovered by distillation at atmospheric pressure. after cooling at 100 ° c, the mixture is washed twice for 3 to 3 times. the unreacted benzaldehyde is recovered by decompression and fractionation. 154 ℃ (1333pa) of the distillate is the finished product.
production method in the presence of alkali conditions, dry distillation castor oil obtained by the aldehyde and benzaldehyde condensation derived. with an aldehyde rate of 80%. in the production conditions, the production of benzaldehyde aldehyde, is to the alkaline solution of methanol to add benzaldehyde, and at about 32 ℃ when the gradual addition of heptaldehyde reaction, until the washing sample after the refraction rate of 1.545 so far. and then add water to the condensation product, separation of alkali methanol water, from which the recovery of methanol. the crude vegetable aldehyde is washed with a salt solution and vacuum distilled to obtain the finished product. suin aldehyde in the air easily oxidized to produce benzoic acid, acetic acid and cinnamic acid. in the air can spontaneous combustion. and sometimes add 0.5% of its amount of diphenylamine as a stabilizer.
production methods from cinnamic acid and amyl alcohol esterification.
production methods benzaldehyde and n-heptaldehyde dissolved in dilute ethanol, sodium hydroxide in the room temperature for two days, the oil was acidified by acetic acid, extracted with ether, dried and then decompression fraction derived.
category flammable liquids
toxic grading poisoning
acute toxicity oral - rat ld50: 3730 mg / kg
stimulate data skin - rabbit 100 mg / 24 h severe
flammability hazardous characteristics flammable; combustion produces irritating smoke
storage and storage characteristics of the warehouse ventilation low temperature drying
fire extinguishing agent dry powder, foam, sand, carbon dioxide
Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)