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- 1H,1H,2H,2H-Perfluorohexan-1-ol
- 1H,1H,2H,2H-Perfluorohexyl bromide
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Cas Database |
| Name |
1H,1H,2H,2H-Perfluorohexan-1-ol |
EINECS | 218-050-9 |
| CAS No. | 2043-47-2 | Density | 1.59 |
| PSA | 20.23000 | LogP | 2.83700 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C6H5 F9 O | Boiling Point | 140-143 ºC |
| Molecular Weight | 264.091 | Flash Point | 164 ºF |
| Transport Information | N/A | Appearance | N/A |
| Safety | 24/25 | Risk Codes | N/A |
| Molecular Structure |
|
Hazard Symbols |
|
| Synonyms |
1,1,2,2-Tetrahydroperfluorohexan-1-ol;1,1,2,2-Tetrahydroperfluorohexyl alcohol; 1H,1H,2H,2H-Nonafluoro-1-hexanol;1H,1H,2H,2H-Nonafluoro-n-hexanol; 1H,1H,2H,2H-Nonafluorohexanol;1H,1H,2H,2H-Perfluorohexan-1-ol; 1H,1H,2H,2H-Perfluorohexanol;2-(Perfluorobutyl)ethanol; 2-(Perfluorobutyl)ethyl alcohol;3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexanol; 3,3,4,4,5,5,6,6,6-Nonafluorohexanol; A1420 |
Article Data | 11 |
1H,1H,2H,2H-Perfluorohexan-1-ol Synthetic route
| Conditions | Yield |
|---|---|
| With hydrogenchloride; formic acid; oxygen; copper; zinc In water at 80℃; for 2h; Product distribution; various solvents, water concentration; | 100% |
| With water In N,N-dimethyl-formamide at 125 - 130℃; under 9000.9 Torr; for 30h; Pressure; Solvent; Green chemistry; | 85% |
| Yield given. Multistep reaction; | |
| With potassium hydroxide In 1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide at 140℃; under 7125.71 Torr; for 10h; Concentration; Solvent; Temperature; |
- 1048684-09-8
potassium 6,6,6,5,5,4,4,3,3-nonafluorohexyl sulfate
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
| Conditions | Yield |
|---|---|
| With hydrogenchloride; water at 70℃; for 25h; pH=0 - 1; | 87% |
- 19430-93-4
3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene
A
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
B
- 116741-81-2
3,3,4,4,5,5,6,6,6-Nonafluoro-2-hexanol
| Conditions | Yield |
|---|---|
| Stage #1: 3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene With bis(cyclohexanyl)borane In tetrahydrofuran at 20℃; for 16h; Stage #2: With dihydrogen peroxide In tetrahydrofuran alkaline solution; Further stages.; |
- 80793-18-6
3-(perfluorohexyl)prop-1-ene
A
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
B
- 80363-03-7
3-(F-hexyl)propan-2-ol
| Conditions | Yield |
|---|---|
| Stage #1: 3-(perfluorohexyl)prop-1-ene With dichloroborane In hexane Stage #2: With dihydrogen peroxide In hexane alkaline solution; Further stages.; |
- 19430-93-4
3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene
A
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
| Conditions | Yield |
|---|---|
| Stage #1: 3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene With benzo[1,3,2]dioxaborole; (η4-cyclooctadiene)((R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl)rhodium(I) tetrfluoroborate In tetrahydrofuran at 0℃; for 1h; Stage #2: With sodium hydroxide; dihydrogen peroxide In ethanol Further stages. Title compound not separated from byproducts.; |
- 19430-93-4
3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene
- 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
A
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
B
- 116741-81-2
3,3,4,4,5,5,6,6,6-Nonafluoro-2-hexanol
| Conditions | Yield |
|---|---|
| Stage #1: 3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; Wilkinson's catalyst In tetrahydrofuran at 20℃; for 2.5h; Stage #2: With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran Further stages. Title compound not separated from byproducts.; |
- 19430-93-4
3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene
- 274-07-7
benzo[1,3,2]dioxaborole
A
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
B
- 116741-81-2
3,3,4,4,5,5,6,6,6-Nonafluoro-2-hexanol
| Conditions | Yield |
|---|---|
| Stage #1: 3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene; benzo[1,3,2]dioxaborole; Wilkinson's catalyst In tetrahydrofuran at 20℃; for 1h; Stage #2: With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran Further stages. Title compound not separated from byproducts.; |
- 2043-55-2
3,3,4,4,5,5,6,6,6-nonafluorohexyliodide
- 2043-57-4
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
- 2043-53-0
2-(n-perfluorooctyl)ethyl iodide
- 2043-54-1
1-iodo-1H,1H,2H,2H-perfluorododecane
- 30046-31-2
1-iodo-1H,1H,2H,2H-perfluorotetradecane
A
- 60699-51-6
1H,1H,2H,2H-perfluorohexadecan-1-ol
B
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
C
- 865-86-1
2-(perfluorodecyl)ethanol
D
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
E
- 39239-77-5
1H,1H,2H,2H-perfluorobutadecan-1-ol
F
- 678-39-7
3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decanol
| Conditions | Yield |
|---|---|
| With water; silver nitrate; copper(II) sulfate at 180℃; Conversion of starting material; Gas phase; |
- 2043-55-2
3,3,4,4,5,5,6,6,6-nonafluorohexyliodide
- 10192-85-5
potassium acrylate
A
- 52591-27-2
perfluorobutylethyl acrylate
B
- 19430-93-4
3,3,4,4,5,5,6,6,6-Nonafluoro-1-hexene
C
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
| Conditions | Yield |
|---|---|
| With 10H-phenothiazine In tert-butyl alcohol at 160℃; for 6h; |
- 2043-47-2
1H,1H,2H,2H-nonafluoro-1-hexanol
- 70887-89-7
3,3,4,4,5,5,6,6,6-nonafluorohexanoic acid
| Conditions | Yield |
|---|---|
| With chromium(VI) oxide; sulfuric acid In diethyl ether; acetone for 0.0833333h; | 98% |
| With chromium(VI) oxide; sulfuric acid In diethyl ether; water; acetone for 0.5h; Jones oxidation; | 81% |
| With Jones reagent In diethyl ether; acetone |
1H,1H,2H,2H-Perfluorohexan-1-ol Chemical Properties
Molecular Structure of 1H,1H,2H,2H-Perfluorohexan-1-ol (CAS NO.2043-47-2):
.gif)
IUPAC Name: 3,3,4,4,5,5,6,6,6-Nonafluorohexan-1-ol
Molecular Formula: C6H5F9O
Molecular Weight: 264.09
EINECS: 218-050-9
XLogP3-AA: 3
H-Bond Donor: 1
H-Bond Acceptor: 10
Index of Refraction: 1.301
Molar Refractivity: 32.71 cm3
Molar Volume: 174.3 cm3
Surface Tension: 16.9 dyne/cm
Density: 1.515 g/cm3
Flash Point: 20.1 °C
Enthalpy of Vaporization: 40.61 kJ/mol
Boiling Point: 109.7 °C at 760 mmHg
Vapour Pressure: 12.9 mmHg at 25 °C
Canonical SMILES: C(CO)C(C(C(C(F)(F)F)(F)F)(F)F)(F)F
InChI: InChI=1S/C6H5F9O/c7-3(8,1-2-16)4(9,10)5(11,12)6(13,14)15/h16H,1-2H2
InChIKey: JCMNMOBHVPONLD-UHFFFAOYSA-N
Product Categories: Organics; Fluorous Chemistry; Fluorous Compounds; Synthetic Organic Chemistry
1H,1H,2H,2H-Perfluorohexan-1-ol Safety Profile
Safety Information of 1H,1H,2H,2H-Perfluorohexan-1-ol (CAS NO.2043-47-2):
Hazard Codes: 
Xi
WGK Germany: 3
Hazard Note: Irritant
1H,1H,2H,2H-Perfluorohexan-1-ol Specification
1H,1H,2H,2H-Perfluorohexan-1-ol (CAS NO.2043-47-2), its Synonyms are 1,1,2,2-Tetrahydroperfluoro-1-hexanol ; 1-Hexanol, 3,3,4,4,5,5,6,6,6-nonafluoro- ; 3,3,4,4,5,5,6,6,6-Nonafluorohexanol ; 1,1,2,2-Tetrahydroperfluorohexyl alcohol ; 3,3,4,4,5,5,6,6,6-Nonafluorohexanol ; 2-(Perfluorobutyl)ethyl alcohol .
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