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Name	2,4-Dichlorobenzotrifluoride	EINECS	206-278-1
CAS No.	320-60-5	Density	1.464 g/cm³
PSA	0.00000	LogP	4.01220
Solubility	8.67mg/L at 25℃	Melting Point	-26 °C
Formula	C₇H₃Cl₂F₃	Boiling Point	193.2 °C at 760 mmHg
Molecular Weight	215.002	Flash Point	78.1 °C
Transport Information	UN 3265 8/PG 2	Appearance	colourless clear liquid
Safety	26-27-36/37/39-45	Risk Codes	34
Molecular Structure		Hazard Symbols	C,Xi
Synonyms	Toluene,2,4-dichloro-a,a,a-trifluoro- (8CI);1,3-Dichloro-4-(trifluoromethyl)benzene;2,4-Dichloro(trifluoromethyl)benzene;2,4-Dichloro-1-(trifluoromethyl)benzene;2,4-Dichloro-a,a,a-trifluorotoluene;2,4-Dichlorobenzotrifluoride;	Article Data	5

2,4-Dichlorobenzotrifluoride Synthetic route

: 7664-39-3
hydrogen fluoride

: 13014-18-1
2,4-dichlorobenzotrichloride

: 320-60-5
2,4-dichloro-benzotrifluoride

Conditions

Conditions	Yield
at 140 - 150℃;
at 140 - 150℃;

: 13014-18-1
2,4-dichlorobenzotrichloride

: 320-60-5
2,4-dichloro-benzotrifluoride

Conditions

Conditions	Yield
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Pressure; Temperature;
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure;
With hydrogen fluoride at 110℃; under 11251.1 - 12751.3 Torr; Temperature; Pressure; Green chemistry;

: 462-06-6
fluorobenzene

: 320-60-5
2,4-dichloro-benzotrifluoride

: 656803-77-9
2,4-dichloro-1-[dichloro-(4-fluorophenyl)methyl]benzene

Conditions

Conditions	Yield
With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 5℃; for 5h;	100%
With aluminium trichloride In 1,2-dichloro-ethane at 0℃; for 5h;
With aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 5℃; for 5h;

: 320-60-5
2,4-dichloro-benzotrifluoride

: 5720-05-8
4-methylphenylboronic acid

: 1419798-74-5
3-chloro-4'-methyl-4-(trifluoromethyl)biphenyl

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere;	97%

: 320-60-5
2,4-dichloro-benzotrifluoride

: 17933-03-8
m-tolylboronic acid

: 1419798-73-4
3-chloro-3'-methyl-4-(trifluoromethyl)biphenyl

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere;	95%

: 320-60-5
2,4-dichloro-benzotrifluoride

: 16419-60-6
2-Methylphenylboronic acid

: 1419798-72-3
3'-chloro-2-methyl-4'-(trifluoromethyl)biphenyl

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 80℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere;	93%

: 320-60-5
2,4-dichloro-benzotrifluoride

: 60933-65-5
(R)-S-methyl-S-phenylsulfoximine

: C14H11NSOClF3

Conditions

Conditions	Yield
Stage #1: 2,4-dichloro-benzotrifluoride; (R)-S-methyl-S-phenylsulfoximine With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate In toluene at 20℃; for 0.5h; Stage #2: In toluene at 135℃; for 1.5h; microwave irradiation; Further stages.;	92%

: 320-60-5
2,4-dichloro-benzotrifluoride

: 400-70-4
2,4-dichloro-5-nitrobenzotrifluoride

Conditions

Conditions	Yield
With sulfuric acid; potassium nitrate at 15 - 20℃; for 18.5h;	87%
With sulfuric acid; nitric acid
Nitrierung;
Nitrierung;

: 75-77-4
chloro-trimethyl-silane

: 320-60-5
2,4-dichloro-benzotrifluoride

: 871254-70-5
[2,6-dichloro-3-(trifluoromethyl)phenyl]trimethylsilane

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran; hexane at -75℃;	82%

: 124-38-9
carbon dioxide

: 320-60-5
2,4-dichloro-benzotrifluoride

: 25922-41-2
2,6-dichloro-3-(trifluoromethyl)benzoic acid

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran; hexane at -75℃;	75%

2,4-Dichlorobenzotrifluoride Chemical Properties

IUPAC Name of o-Aminotrifluoromethylbenzene (320-60-5): 2,4-dichloro-1-(trifluoromethyl)benzene
Product Categories: Chlorine Compounds;Fluorine Compounds
Molecular Formula: C₇H₃Cl₂F₃
Molecular Weight: 214.99993
Appearance:colourless clear liquid
Surface Tension: 27.4 dyne/cm
Index of Refraction: 1.47
odor: penetrating
BRN: 2098743
Melting Point: -26 °C
Density: 1.464 g/cm³
Flash Point: 78.1 °C
Enthalpy of Vaporization: 41.18 kJ/mol
Boiling Point: 193.2 °C at 760 mmHg
Vapour Pressure: 0.656 mmHg at 25 °C
CAS DataBase Reference:320-60-5(CAS DataBase Reference)
NIST Chemistry Reference:320-60-5(NIST)
EPA Substance Registry System:320-60-5(EPA Substance)
Synonyms of o-Aminotrifluoromethylbenzene (320-60-5):
2,4-dichloro-1-(trifluoromethyl)-benzen;2,4-dichloro-alpha,alpha,alpha-trifluoro-toluen;2,4-Dichlorotrifluoromethylbenzene;1,3-DICHLORO-4-(TRIFLUOROMETHYL)BENZENE;2,4-Dichloro-1-(triflouromethyl)-benzene;2,4-DICHLORO-1-(TRIFLUOROMETHYL)BENZENE;2,4-DCBTF;2,4-DICHLORO-A,A,A-TRIFLUOROTOLUENE; 2,4-Dichlorobenzotrifluoride;2,4-Dichloro-1-(trifluoromethyl)benzene;Benzene, 2,4-dichloro-1-(trifluoromethyl)-;2,4-Dichloro-alpha,alpha,alpha-trifluorotoluene;Toluene, 2,4-dichloro-alpha,alpha,alpha-trifluoro-

2,4-Dichlorobenzotrifluoride Uses

o-Aminotrifluoromethylbenzene (320-60-5) is raw material of madinitramine which is weedicide used in the dry soil.

2,4-Dichlorobenzotrifluoride Production

o-Aminotrifluoromethylbenzene(320-60-5) is synthesized by the method of chloridizing parachlorotoluene.

2,4-Dichlorobenzotrifluoride Safety Profile

Safety Information of o-Aminotrifluoromethylbenzene(320-60-5):
Hazard Codes:C ,Xi
Risk Statements:34
34:Causes burns
Safety Statements:26-27-36/37/39-45
26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
27:Take off immediately all contaminated clothing
36/37/39:Wear suitable protective clothing, gloves and eye/face protection
45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
RIDADR:UN 3265 8/PG 2
WGK Germany:2
RTECS:CZ5566877
Hazard Note:Corrosive
TSCA:T
HazardClass:8
PackingGroup:III

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