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2,6-DIIODO-4-NITROPHENOL

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Name

2,6-DIIODO-4-NITROPHENOL

EINECS 206-170-4
CAS No. 305-85-1 Density 2.717 g/cm3
PSA 66.05000 LogP 3.03280
Solubility very sparingly soluble in water Melting Point 152-154 °C(lit.)
Formula C6H3I2NO3 Boiling Point 310.6 °C at 760 mmHg
Molecular Weight 390.904 Flash Point 141.6 °C
Transport Information UN 2811 6.1/PG 3 Appearance yellow crystalline solid
Safety 26-28-36/37/39-45-28A Risk Codes 20/21/22-36/37/38-25
Molecular Structure Molecular Structure of 305-85-1 (2,6-Diiodo-4-nitrophenol) Hazard Symbols HarmfulXn, ToxicT
Synonyms

4-Nitro-2,6-diiodophenol;Ancylol;Disofen;Disophenol;Iodofen;Iodophen;Syngamix;

Article Data 39

2,6-DIIODO-4-NITROPHENOL Synthetic route

100-02-7

4-nitro-phenol

305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With hydrogenchloride; potassium iodate; potassium iodide In methanol; water at 20℃;99%
With sodium periodate; sulfuric acid; iodine; potassium iodide; sodium sulfite In water; acetic acid at 25℃; for 4h;98%
With N-iodo-S-methyl-S-phenyl sulfoximine; acetic acid at 22℃; for 3h; Sealed tube;98%
100-02-7

4-nitro-phenol

A

305-85-1

2,6-diiodo-4-nitrophenol

B

89487-91-2

2-iodo-4-nitrophenol

Conditions
ConditionsYield
With iodine; silver sulfate In ethanol at 20℃; for 0.5h;A 22%
B 50%
With sulfuric acid; dihydrogen peroxide; potassium iodide In methanol at 60℃; for 2h;A 18%
B 42%
With iodine; silver nitrate In acetonitrile for 2h; Ambient temperature;A 5%
B 12%
636-98-6

p-nitrobenzene iodide

A

100-25-4

para-dinitrobenzene

B

305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With sodium nitrite
609-23-4

2,4,6-Triiodophenol

A

305-85-1

2,6-diiodo-4-nitrophenol

B

20294-48-8

diiodo-4,6 nitro-2 phenol

Conditions
ConditionsYield
With acetic acid; sodium nitrite; benzene Trennung durch fraktionierte Krystallisation der Kaliumsalze;
With acetic acid; sodium nitrite; benzene
616-59-1

2-hydroxyl-5-nitrobenzenesulfonic acid

A

305-85-1

2,6-diiodo-4-nitrophenol

B

2-hydroxy-3-iodo-5-nitro-benzenesulfonic acid

Conditions
ConditionsYield
With ethanol; iodine; mercury(II) oxide
96-97-9

5-nitrosalicylic acid

305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With iodine; mercury(II) oxide
96-97-9

5-nitrosalicylic acid

A

305-85-1

2,6-diiodo-4-nitrophenol

B

861565-06-2

2-hydroxy-3-iodo-5-nitro-benzoic acid

Conditions
ConditionsYield
With ethanol; iodine; mercury(II) oxide
28177-54-0

2,6-diiodo-phenol

305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
durch Nitrierung;
28177-54-0

2,6-diiodo-phenol

A

305-85-1

2,6-diiodo-4-nitrophenol

B

13073-26-2

2-iodo-6-nitro-phenol

Conditions
ConditionsYield
With nitric acid
16825-79-9

1-iodyl-4-nitrobenzene

305-85-1

2,6-diiodo-4-nitrophenol

Conditions
ConditionsYield
With sodium nitrite
With sodium azide

2,6-DIIODO-4-NITROPHENOL Chemical Properties

Empirical Formula: C6H3I2NO3
Molecular Weight: 390.9019 
IUPAC Name: 2,6-Diiodo-4-nitrophenol
Synonyms: Phenol, 2,6-diiodo-4-nitro- ; Disofen ; Diisophenol ; Ancylol
Melting Point: 152-154 °C(lit.)
Flash Point: 141.6 °
Boiling Point: 310.6 °C at 760 mmHg
Density of 2,6-Diiodo-4-nitrophenol (305-85-1): 2.717 g/cm
Vapour Pressure: 0.000325 mmHg at 25°C
Index of Refraction: 1.782 
Water Solubility: 2,6-Diiodo-4-nitrophenol (305-85-1) is very sparingly soluble
Sensitive: Light Sensitive
Stability: 2,6-Diiodo-4-nitrophenol (305-85-1) is stable.
Appearance: 2,6-Diiodo-4-nitrophenol (305-85-1) is a yellow crystalline solid

2,6-DIIODO-4-NITROPHENOL Uses

 2,6-Diiodo-4-nitrophenol (305-85-1) is used against hookworm.

2,6-DIIODO-4-NITROPHENOL Toxicity Data With Reference

1.    

orl-rat LD50:170 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
2.    

ipr-rat LD50:105 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
3.    

scu-rat LD50:122 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
4.    

ivn-rat LD50:105 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
5.    

orl-mus LD50:212 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
6.    

ipr-mus LD50:107 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
7.    

scu-mus LD50:110 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
8.    

ivn-mus LD50:88 mg/kg

    TXAPA9    Toxicology and Applied Pharmacology. 6 (1964),232.
9.    

par-uns LDLo:36 mg/kg

    FAZMAE    Fortschritte der Arzneimittelforschung. 17 (1973),108.

2,6-DIIODO-4-NITROPHENOL Consensus Reports

Reported in EPA TSCA Inventory.

2,6-DIIODO-4-NITROPHENOL Safety Profile

Poison by ingestion, intraperitoneal, subcutaneous, intravenous, and parenteral routes. An anthelmintic. When heated to decomposition it emits very toxic fumes of I and NOx. See also NITRO COMPOUNDS of AROMATIC HYDROCARBONS.
Safety: DANGER: POISON, causes cyanosis; skin, eye, lung irritation. Safety glasses, good ventilation.
Hazard Codes: Xn: Harmful ,
T: Toxic
Risk Statements: 20/21/22: Harmful by inhalation, in contact with skin and if swallowed
36/37/38: Irritating to eyes, respiratory system and skin
25: Toxic if swallowed 
Safety Statements: 26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
28: After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer)
36/37/39: Wear suitable protective clothing, gloves and eye/face protection
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
RIDADR  UN 2811 6.1/PG 3
WGK Germany: 3
RTECS: SL0750000
HazardClass: 6.1
PackingGroup: III

2,6-DIIODO-4-NITROPHENOL Specification

 2,6-Diiodo-4-nitrophenol (305-85-1) is a yellow crystalline solid used against hookworm. It is a halogenated and nitrated phenol. Reacts as a weak acid. It is stable and very sparingly soluble in water.

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