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Name	2,6-Dichloroaniline	EINECS	210-160-5
CAS No.	608-31-1	Density	1.401 g/cm³
PSA	26.02000	LogP	3.15680
Solubility	1.6 g/L (20 °C) in water	Melting Point	36-38 °C(lit.)
Formula	C₆H₅Cl₂N	Boiling Point	219.9 °C at 760 mmHg
Molecular Weight	162.018	Flash Point	86.8 °C
Transport Information	UN 3442 6.1/PG 2	Appearance	white to brown crystalline solid
Safety	28-36/37-45-60-61-28A	Risk Codes	23/24/25-33-50/53
Molecular Structure		Hazard Symbols	T, N, Xi
Synonyms	Aniline,2,6-dichloro- (7CI,8CI);2,6-Dichlorobenzenamine;2,6-Dichlorophenylamine;	Article Data	39

2,6-Dichloroaniline Synthetic route

: 22134-75-4
4-amino-3,5-dichloro-benzenesulfonamide

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With sulfuric acid at 180℃;	96.2%

: 601-88-7
2,6-dichloronitrobenzene

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With ammonium formate at 20℃; for 0.75h; Reduction;	91%
With hydrogenchloride; tin
With hydrogen; silver; silica gel In ethanol at 140℃; under 15001.2 Torr; for 3h;	100 % Chromat.

: 697-88-1
4-bromo-2,6-dichloroaniline

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With methanol; gold; hydrogen; caesium carbonate at 100℃; under 3800.26 Torr; for 72h;	91%
With hydrogen bromide; acetic acid; aniline for 24h; Heating;	86%
With hydrogen bromide; acetic acid; aniline Reflux;	80%

: 56961-25-2
4-amino-3,5-dichlorobenzoic acid

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With copper(I) oxide In quinoline at 220℃; for 6h; Autoclave;	85%
In water	80%

: 10286-88-1
N-(2,6-dichlorophenyl)benzamide

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With sulfuric acid for 3h; Heating;	68%

: 87-65-0
2,6-Dichlorophenol

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With potassium carbonate; potassium iodide; Chloroacetamide In N,N-dimethyl-formamide at 90 - 150℃; for 4h; Reagent/catalyst; Smiles Aromatic Rearrangement;	65%

: 95-51-2
2-Chloroaniline

A: 554-00-7
2,4-Dichloroaniline

B: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With chlorine In chlorobenzene at 15℃; for 6h; Solvent; Reagent/catalyst; Temperature;	A 60% B 35%

: 62-53-3
aniline

A: 554-00-7
2,4-Dichloroaniline

B: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With hydrogenchloride; potassium permanganate In acetonitrile at 60℃;	A 19% B 29%

: 515-74-2
sodium sulfanilate

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With carbon dioxide; water; chlorine Behandeln des Reaktionsprodukts mit 98 prozentiger Schwefelsaeure und Dampf bei 180grad;

: 56700-68-6
tert-butyl (2,6-dichlorophenyl)carbamate

: 608-31-1
2,6-Dichloroaniline

Conditions

Conditions	Yield
With hydrogenchloride In ethanol

2,6-Dichloroaniline Chemical Properties

Molecular Formula:C₆H₅Cl₂N
Molar mass:162.0166 g/mol
Structure of 2,6-Dichloroaniline(608-31-1):

Synonyms of 2,6-Dichloroaniline(608-31-1):2,6-dichlorobenzenamine;2,6-Dichloranilin;2,6-DICHLOROANILINE;Benzenamine, 2,6-dichloro-
Density:1.401 g/cm³
Flash Point:118 °C
Boiling Point:228°C
Index of Refraction:1.613
Vapour Pressure: 0.116 mmHg at 25°C
Melting point:35-39°C
Water solubility: 1.6 g/L (20 °C)

2,6-Dichloroaniline Uses

2,6-Dichloroaniline(608-31-1) can be used in the pharmaceutical industry for the synthesis of antibacterial agents of lomefloxacin, Lee uric acid and clonidine.
2,6-Dichloroaniline(608-31-1) also can be used in the pesticide industry for the synthesis of herbicides and fungicides.

2,6-Dichloroaniline Production

1. the right-amino benzene sulfonamide as the raw , chloride by concentrated hydrochloric acid, sulfuric acid hydrolysis and then derived .
2. For amino acid ester method: by chlorination, the water decarboxylation derived.
3. For amino acid method.

2,6-Dichloroaniline Toxicity Data With Reference

Carcinogenicity:2,6-Dichloroaniline(608-31-1)- Not listed as a carcinogen by IARC, NTP,ACGIH, or CA Prop 65.
Other: See actual entry in RTECS for complete information.

2,6-Dichloroaniline Safety Profile

Hazard Codes:T

,Xi

Risk Statements:
23: Toxic by inhalation
24: Toxic in contact with skin
25: Toxic if swallowed
30: Can become highly flammable in use
50: Very Toxic to aquatic organisms
53: May cause long-term adverse effects in the aquatic environment
Safety Statements:
28: After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer)
36: Wear suitable protective clothing
37: Wear suitable gloves
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
60: This material and/or its container must be disposed of as hazardous waste
61: Avoid release to the environment. Refer to special instructions safety data sheet

2,6-Dichloroaniline Specification

Stability and Reactivity of 2,6-Dichloroaniline(608-31-1):
Conditions to Avoid: Incompatible materials, light, exposure to air.
Chemical Stability:Stable under normal temperatures and pressures.
Incompatibilities with Other Materials: Exposure to acids, acid chlorides, acid anhydrides,air.
Hazardous Decomposition Products: carbon dioxide,carbon monoxide,Hydrogen chloride,nitrogen oxides.

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