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2-Amino-5-bromine-2'-chloro benzophenone

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Name

2-Amino-5-bromine-2'-chloro benzophenone

EINECS N/A
CAS No. 60773-49-1 Density 1.568 g/cm3
PSA 43.09000 LogP 4.49690
Solubility N/A Melting Point 85-87°C
Formula C13H9BrClNO Boiling Point 456.2 °C at 760 mmHg
Molecular Weight 310.578 Flash Point 229.7 °C
Transport Information N/A Appearance yellow crystal powder
Safety Risk Codes N/A
Molecular Structure Molecular Structure of 60773-49-1 (2-Amino-5-bromine-2'-chloro benzophenone) Hazard Symbols N/A
Synonyms

5-Bromo-2'-chloro-2-aminobenzophenone;

Article Data 5

2-Amino-5-bromine-2'-chloro benzophenone Synthetic route

39263-32-6

2-amino-5-bromobenzonitrile

3900-89-8

2-Chlorobenzeneboronic acid

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

Conditions
ConditionsYield
With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate In 2-methyltetrahydrofuran; water at 80℃; for 36h;58%
609-65-4

o-chlorobenzoyl chloride

106-40-1

4-bromo-aniline

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

Conditions
ConditionsYield
Stage #1: o-chlorobenzoyl chloride; 4-bromo-aniline at 0 - 120℃; for 1h;
Stage #2: With zinc(II) chloride at 120 - 195℃; for 3h;
Stage #3: With hydrogenchloride; sulfuric acid; water more than 3 stages;
37%
(i) ZnCl2, (ii) aq. HCl, (iii) H2SO4; Multistep reaction;
70030-11-4

3-hydroxy-7-bromo-5-(2'-chlorophenyl)-1,2-dihydro-3H-1,4-benzodiazepin-2-one

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

Conditions
ConditionsYield
With hydrogenchloride for 0.5h; boiling water bath;
51753-57-2

phenazepam

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

Conditions
ConditionsYield
With hydrogenchloride for 0.5h; boiling water bath;
6780-38-7

N-phthaloylglycine chloride

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

87213-48-7

5-bromo-2'-chloro-2-(phthalimidoacetamido)benzophenone

Conditions
ConditionsYield
In chloroform for 5h; Heating;97%
60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

89445-68-1

2-amino-5-bromo-4'-chlorobenzhydrol

Conditions
ConditionsYield
With sodium tetrahydroborate In water at 25 - 30℃; for 2h;96%
60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

C(14)CH4ClNO*ClH

3-[14C]-7-bromo-5-(o-chlorophenyl)-1,2-dihydro-3H-1,4-benzodiazepin-2-one

Conditions
ConditionsYield
Condensation;90%
773837-37-9

sodium cyanide

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

17562-66-2

4-amino-3-(2-chlorobenzoyl)benzonitrile

Conditions
ConditionsYield
With copper(l) iodide; potassium iodide; N,N`-dimethylethylenediamine In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 16h; Inert atmosphere;76%
537-47-3

4-phenyl-semicarbazide

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

A

C20H16BrClN4O

B

C20H16BrClN4O

Conditions
ConditionsYield
With hydrogenchloride In ethanol for 5h;A 35%
B 21%
598-21-0

2-Bromoacetyl bromide

60773-49-1

(2-amino-5-bromophenyl)(2-chlorophenyl)methanone

32711-85-6

5-bromo-2-(2-bromo-acetylamino)-2'-chloro-benzophenone

Conditions
ConditionsYield
With pyridine

2-Amino-5-bromine-2'-chloro benzophenone Chemical Properties

Molecular Structure of Methanone,(2-amino-5-bromophenyl)(2-chlorophenyl)- (CAS NO.60773-49-1):

Molecular Formula: C13H9BrClNO
Molecular Weight: 310.5737
IUPAC Name: (2-Amino-5-bromophenyl)-(2-chlorophenyl)methanone
Synonyms of Methanone,(2-amino-5-bromophenyl)(2-chlorophenyl)- (CAS NO.60773-49-1): 5-Bromo-2'-chloro-2-aminobenzophenone ; BCABP
CAS NO: 60773-49-1
Classification Code: Aromatic Benzophenones & Derivatives (substituted) 
Index of Refraction: 1.657
Molar Refractivity: 72.86 cm3
Molar Volume: 197.9 cm3
Surface Tension: 54.9 dyne/cm
Density: 1.568 g/cm3
Flash Point: 229.7 °C
Enthalpy of Vaporization: 71.61 kJ/mol
Boiling Point: 456.2 °C at 760 mmHg
Vapour Pressure of Methanone,(2-amino-5-bromophenyl)(2-chlorophenyl)- (CAS NO.60773-49-1): 1.65E-08 mmHg at 25°C

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