- 5-Bromoindole-2-carboxylic acid
- 5-Bromoindole-2-carboxylic acid methyl ester
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Cas Database |
| Name |
5-Bromoindole-2-carboxylic acid |
EINECS | N/A |
| CAS No. | 7254-19-5 | Density | 1.828 g/cm3 |
| PSA | 53.09000 | LogP | 2.62860 |
| Solubility | N/A | Melting Point |
287-288 °C |
| Formula | C9H6BrNO2 | Boiling Point | 470.932 °C at 760 mmHg |
| Molecular Weight | 240.056 | Flash Point | 238.611 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | 26-37/39 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 Xi
|
| Synonyms |
5-bromo-1H-indole-2-carboxylic acid; |
Article Data | 12 |
5-Bromoindole-2-carboxylic acid Synthetic route
- 16732-70-0
ethyl 5-bromoindolecarboxylate
- 7254-19-5
5-bromo-2-indolecarboxylic acid
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 110℃; for 0.0333333h; Microwave irradiation; | 95% |
| With sodium hydroxide In ethanol; water at 70℃; for 2h; | 92% |
| Stage #1: ethyl 5-bromoindolecarboxylate With sodium hydroxide In methanol; water for 0.5h; Reflux; Green chemistry; Stage #2: With hydrogenchloride In methanol; water at 40℃; pH=3 - 4; Green chemistry; | 91% |
- 17403-17-7
(5-bromo-2-nitro-phenyl)-pyruvic acid
- 7254-19-5
5-bromo-2-indolecarboxylic acid
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; iron(II) hydroxide |
- 7254-19-5
5-bromo-2-indolecarboxylic acid
| Conditions | Yield |
|---|---|
| With potassium hydroxide | |
| With sodium hydroxide |
| Conditions | Yield |
|---|---|
| With ammonium hydroxide; iron(II) sulfate |
| Conditions | Yield |
|---|---|
| With 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate In N,N-dimethyl-formamide at 105℃; for 4h; |
- 16382-11-9
ethyl 2-[2-(4-bromophenyl)hydrazinylidene]propanoate
- 7254-19-5
5-bromo-2-indolecarboxylic acid
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: phosphoric acid / 1.33 h / 80 - 100 °C / Green chemistry 2.1: sodium hydroxide / water; methanol / 0.5 h / Reflux; Green chemistry 2.2: 40 °C / pH 3 - 4 / Green chemistry View Scheme |
- 67-56-1
methanol
- 7254-19-5
5-bromo-2-indolecarboxylic acid
- 210345-56-5
5-bromo-1H-indole-2-carboxylic acid methyl ester
| Conditions | Yield |
|---|---|
| With sulfuric acid Inert atmosphere; Reflux; | 98% |
| With thionyl chloride at 65℃; for 2.33333h; Cooling; Inert atmosphere; | 96% |
| With sulfuric acid | 96% |
- 7254-19-5
5-bromo-2-indolecarboxylic acid
- 124-40-3
dimethyl amine
- 1246250-21-4
5-bromo-1H-indole-2-carboxylic acid dimethylamide
| Conditions | Yield |
|---|---|
| With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 16h; | 96% |
| Stage #1: 5-bromo-2-indolecarboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: dimethyl amine In tetrahydrofuran at 20℃; for 16h; | 96% |
- 7254-19-5
5-bromo-2-indolecarboxylic acid
- 22483-09-6
2,2-dimethoxyethylamine
| Conditions | Yield |
|---|---|
| With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 25℃; for 2h; | 96% |
- 123-75-1
pyrrolidine
- 7254-19-5
5-bromo-2-indolecarboxylic acid
- 1246250-06-5
(5-bromo-1H-indol-2-yl)-pyrrolidin-1-yl-methanone
| Conditions | Yield |
|---|---|
| With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 17h; Inert atmosphere; | 95% |
| Stage #1: 5-bromo-2-indolecarboxylic acid With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran; water for 0.166667h; Stage #2: pyrrolidine at 20℃; for 17h; Inert atmosphere; | 95% |
5-Bromoindole-2-carboxylic acid Chemical Properties
Molecular formula: C9H6BrNO2
Molecular Weight: 240.05
Molecular Structure :
Melting point: 287-288
storage temp.: -20°C
5-Bromoindole-2-carboxylic acid Safety Profile
Hazard Codes: 
Xi
Hazard Note: Irritant
The Risk Statements information of 5-Bromoindole-2-carboxylic acid:
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of 5-Bromoindole-2-carboxylic acid:
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
37/39: Wear suitable gloves and eye/face protection
WGK Germany: 3
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