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6,6-DIMETHYL-2-NORPINENE-2-ETHANOL

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Name

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL

EINECS N/A
CAS No. 128-50-7 Density 0.978g/cm3
PSA 20.23000 LogP 2.36120
Solubility N/A Melting Point N/A
Formula C11H18 O Boiling Point 235°Cat760mmHg
Molecular Weight 166.263 Flash Point 98.9°C
Transport Information N/A Appearance N/A
Safety Moderately toxic by ingestion and intramuscular routes. A skin irritant. When heated to decomposition it emits acrid smoke and irritating fumes. Risk Codes 22
Molecular Structure Molecular Structure of 128-50-7 (NOPOL) Hazard Symbols
Synonyms

2-Norpinene-2-ethanol,6,6-dimethyl- (6CI,7CI,8CI); 10-(Hydroxymethyl)-2-pinene;2-(6,6-Dimethylbicyclo[3.1.1]hept-2-en-2-yl)ethanol;6,6-Dimethyl-2-norpinene-2-ethanol;6,6-Dimethylbicyclo[3.1.1]hept-2-ene-2-ethanol; Homomyrtenol; NSC 1284; NSC404962; Nopol; Nopol (terpene)

Article Data 26

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL Synthetic route

50-00-0

formaldehyd

177698-19-0

Beta-pinene

Conditions
ConditionsYield
With iron(III) phosphate In acetonitrile at 80℃; for 4h; Prins condensation;100%
With mesoporous SnSBA-15(5) In toluene at 89.84℃; for 6h; Prins reaction;96.7%
at 150℃;61%

benzyl nopyl ether

Conditions
ConditionsYield
With hydrogen; benzyl bromide; Pd<*>MCM-48 In methanol under 760.051 Torr;95%
With Na2K-SG(I) In tetrahydrofuran at 20℃; Inert atmosphere;
77661-66-6

2-<2-(methoxymethoxy)ethyl>-6,6-dimethylbicyclo<3.1.1>hept-2-ene

Conditions
ConditionsYield
zirconium(IV) chloride In isopropyl alcohol for 4h; Heating;93%

tert-butyl-[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-en-2-yl)-ethoxy]-dimethyl-silane

Conditions
ConditionsYield
With zirconium(IV) chloride In acetonitrile at 20℃; for 0.333333h;87%
128-51-8

nopyl acetate

Conditions
ConditionsYield
With lithium aluminium tetrahydride86%
(saponification);
69978-56-9

[2-(6,6-Dimethyl-bicyclo[3.1.1]hept-2-en-2-yl)-ethoxy]-trimethyl-silane

Conditions
ConditionsYield
With tris paraperiodate In benzene for 0.166667h; Heating;85%
693272-53-6

4-{[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-en-2-yl)-ethoxy]-phenyl-methyl}-biphenyl

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane at 20℃; for 7h;83%
693272-54-7

4-{[2-(6,6-dimethyl-bicyclo[3.1.1]hept-2-en-2-yl)-ethoxy]-diphenyl-methyl}-biphenyl

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 3h;82%

6,6-dimethyl-2-[2-(3-methyl-but-2-enyloxy)-ethyl]-bicyclo[3.1.1]hept-2-ene

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; water at 20℃; for 1.5h;78%
Conditions
ConditionsYield
With Cr and Fe containing metal organic framework MIL-101; air In acetonitrile at 80℃; for 30h; Catalytic behavior; Reagent/catalyst;A 63.75%
B 21.25%

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL Chemical Properties

IUPAC Name: 2-(7,7-Dimethyl-4-bicyclo[3.1.1]hept-3-enyl)ethanol
Synonyms: NOPOL ; 2-(6,6-Dimethylbicyclo[3.1.1]hept-2-en-2-yl)ethanol ; 6,6-Dimethyl-2-(2-hydroxyethyl)-2-norpinene ; 6,6-Dimethyl-2-norpinene-2-ethano ; 6,6-Dimethylbicyclo-(3.1.1)-2-heptene-2-ethanol ; 6,6-Dimethyl-bicyclo[3.1.1]hept-2-ene-2-ethano ; Bicyclo[3.1.1]hept-2-ene-2-ethanol, 6,6-dimethyl- ; Homomyretenol
CAS NO: 128-50-7
Molecular Formula of 6,6-Dimethyl-2-norpinene-2-ethano (CAS NO.128-50-7) : C11H18O
Molecular Weight of 6,6-Dimethyl-2-norpinene-2-ethano (CAS NO.128-50-7) :166.26
Molecular Structure of 6,6-Dimethyl-2-norpinene-2-ethano (CAS NO.128-50-7) :
EINECS: 204-890-3
Mol File: 128-50-7.mol
Index of Refraction: 1.501
Surface Tension: 32.1 dyne/cm
Density: 0.978 g/cm3
Flash Point: 98.9 °C
Enthalpy of Vaporization: 54.83 kJ/mol
Boiling Point: 235 °C at 760 mmHg
Vapour Pressure: 0.00937 mmHg at 25°C

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL Toxicity Data With Reference

1.    

skn-rbt 500 mg/24H MOD

    FCTXAV    Food and Cosmetics Toxicology. 17 (1979),879.
2.    

orl-rat LD50:890 mg/kg

    FCTXAV    Food and Cosmetics Toxicology. 17 (1979),879.
3.    

ims-mus LD50:500 mg/kg

    JSICAZ    Journal of Scientific and Industrial Research, Section C: Biological Sciences. 21 (1962),342.

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL Consensus Reports

Reported in EPA TSCA Inventory.

6,6-DIMETHYL-2-NORPINENE-2-ETHANOL Safety Profile

Hazard Codes HarmfulXn
Risk Statements 22
R22: 6,6-Dimethyl-2-norpinene-2-ethano (CAS NO.128-50-7) is harmful if swallowed.

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