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Cas Database

Name	Boc-D-Phenylglycine	EINECS	1533716-785-6
CAS No.	33125-05-2	Density	1.182 g/cm³
PSA	66.84000	LogP	2.51270
Solubility	Insoluble in water. Slightly soluble in DMSO and methanol.	Melting Point	88-91 °C
Formula	C₁₃H₁₇NO₄	Boiling Point	407.2 °C at 760 mmHg
Molecular Weight	251.282	Flash Point	200.1 °C
Transport Information	N/A	Appearance	N/A
Safety	24/25	Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	Benzeneaceticacid, a-[[(1,1-dimethylethoxy)carbonyl]amino]-,(R)-;(R)-N-Boc-2-amino-2-phenylaceticacid;(R)-[(tert-Butoxycarbonyl)amino]phenylethanoicacid;BOC-D-Phg-OH;D-2-tert-Butoxycarboxamido-2-phenylacetic acid;N-(tert-Butoxycarbonyl)-D-2-phenylglycine;N-tert-Butyloxycarbonyl-D-phenylglycine;	Article Data	77

Boc-D-Phenylglycine Synthetic route

: 24424-99-5
di-tert-butyl dicarbonate

: 875-74-1
(R)-phenylglycine

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With sodium hydroxide In tert-butyl alcohol at 20℃; for 1h; Inert atmosphere;	100%
With potassium hydrogencarbonate In tetrahydrofuran; water for 18h;	99%
With sodium hydroxide	96%

: 875-74-1
(R)-phenylglycine

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With triethylamine In 1,4-dioxane; water for 18h;	94%

: 875-74-1
(R)-phenylglycine

: tert-butyl (2,4-dioxo-3-azaspiro[5,5]undecan-3-yl) carbonate

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With sodium carbonate In 1,4-dioxane; water at 25℃; for 12h;	89%

: 956101-46-5
tert-butyl [(1S)-1-phenylprop-2-en-1-yl]imidocarbonate

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With ruthenium trichloride; sodium periodate In tetrachloromethane; water; acetonitrile	85%

: 875-74-1
(R)-phenylglycine

: 50739-44-1
1-(t-butoxycarbonyl)-1,2,4-triazolo<4,3-a>pyridinium-3-olate

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With sodium hydroxide In acetone for 2h; Ambient temperature;	84%

: 2900-27-8, 3601-66-9, 14675-97-9, 33125-05-2
2-(tert-butoxycarbonylamino)-2-phenylacetic acid

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
	82%

: 125414-45-1
(2R,3R)-3-<(tert-butoxycarbonyl)amino>-3-phenyl-1,2-propanediol

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With ruthenium trichloride; sodium periodate; sodium carbonate In tetrachloromethane; water; acetonitrile for 2h; Ambient temperature;	79%

: 67341-01-9, 117049-14-6, 138457-46-2, 102089-74-7
(R)-N-(tert-butoxycarbonyl)phenylglycinol

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
With ruthenium trichloride; sodium periodate In tetrachloromethane; water; acetonitrile at 0 - 20℃; for 1h;	77%
With dipyridinium dichromate In N,N-dimethyl-formamide Ambient temperature;
With dipyridinium dichromate In N,N-dimethyl-formamide for 6h; Ambient temperature;

: C16H17F6NO4

A: 33125-05-2
Boc-D-Phg-OH

B: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

Conditions

Conditions	Yield
With C28H30N3O2(1+)*Br(1-); sodium hydroxide In chloroform at 0℃; for 24h;	A n/a B 35%

: 124-38-9
carbon dioxide

: 186375-61-1
N-(triisopropylsilyl)-N-(tert-butyloxycarbonyl)benzylamine

: 33125-05-2
Boc-D-Phg-OH

Conditions

Conditions	Yield
Stage #1: N-(triisopropylsilyl)-N-(tert-butyloxycarbonyl)benzylamine With sec.-butyllithium; (-)-sparteine In diethyl ether; cyclohexane at -78℃; for 3h; Stage #2: carbon dioxide In diethyl ether; cyclohexane for 0.333333h;	7%

Boc-D-Phenylglycine Chemical Properties

The Molecular formula of Boc-D-Phg-OH(33125-05-2): C₁₃H₁₇NO₄
The Molecular Weight of Boc-D-Phg-OH(33125-05-2): 251.2784
The Molecular Structure of Boc-D-Phg-OH(2900-27-8):

Index of Refraction: 1.532
Molar Refractivity: 65.86 cm³
Molar Volume: 212.5 cm³
Polarizability: 26.11 10 ^-24 cm³
Surface Tension: 45.2 dyne/cm
Boiling Point: 407.2 °C at 760 mmHg
Density: 1.182 g/cm³
Flash Point: 200.1 °C
Enthalpy of Vaporization: 69.49 kJ/mol
Vapour Pressure: 2.32E-07 mmHg at 25°C

Boc-D-Phenylglycine Safety Profile

The Safety Statements information of Boc-D-Phg-OH(33125-05-2):
24/25: Avoid contact with skin and eyes
WGK Germany: 3

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