Synthesis and characterization of donor-functionalized N,S-compounds containing the ortho -aminothiophenol motif
A series of twenty S-benzyl ortho-aminothiophenol and S,S-xylylene-bridged bis(ortho-aminothiophenol) compounds and their imine derivatives have been synthesized in moderate to excellent yields and characterized. The syntheses were optimized, including large-scale syntheses, and an improved purification method involving the HCl salt was developed. This paper also serves as a comprehensive review of xylylene-bridged bis(ortho-aminothiophenol) compounds. Georg Thieme Verlag Stuttgart New York.
Cross, Edward D.,Shehzad, Usman A.,Lloy, Samantha M.,Brown, Adam R. C.,Mercer, Todd D.,Foster, Daniel R.,McLellan, Beth L.,Murray, Alexander R.,English, Margaret A.,Bierenstiel, Matthias
experimental part
p. 303 - 315
(2011/03/18)
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