Copper(I) mediated acylation of trifluorovinyl zinc reagents. The preparation of trifluorovinyl ketones
Copper(I) mediated acylation of trifluorovinyl zinc in glyme solvents with aliphatic carboxylic acid chlorides provides a facile preparative route to trifluorovinyl ketones .These ketones exhibit two carbonyl bands in the FT-IR spectrum, which were assigned to the S-cis and S-trans conformers.Calculations support the conformer assignments.
Spawn, Terence D.,Burton, Donald J.
p. 876 - 880
(2007/10/02)
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