cas 111306-36-6, Pyrimido[1,2-a]benzimidazol-2-amine, 4-methyl- (9CI) | Articles data ｜lookchem

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111306-36-6

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CYCLOCONDENSATION OF (BENZIMIDAZOL-2-YL)CYANAMIDE WITH ACETYLACETONE IN THE PRESENCE OF NICKEL ACETYLACETONATE
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Dorokhov, V. A.,Gordeev, M. F.
p. 418
(1987)
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SYNTHESIS OF FUNCTIONALIZED PYRIMIDOBENZIMIDAZOLES FROM (BENZIMIDAZOL-2-YL)CYANAMIDE AND β-DICARBONYL COMPOUNDS USING NICKEL COMPLEXES OR SALTS
It was found that cyclocondensation of (benzimidazol-2-yl)cyanamide with β-diketones and β-ketoesters proceeds in the presence of β-ketoenolates or nickel(2+) acetate with the formation of 2-aminopyrimidobenzimidazole derivatives.Protonation (deute
Dorokhov, V. A.,Gordeev, M. F.,Dem'yanets, Z. K.,Bochkareva, M. N.,Bogdanov, V. S.
p. 2354 - 2362
(2007/10/02)

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Chemical Properties

Melting Point: 319-320 °C(Solv: acetonitrile (75-05-8))
Boiling Point: 364.3±42.0 °C(Predicted)
Density: 1.41±0.1 g/cm3(Predicted)
PKA: 6.79±0.30(Predicted)
PSA: 56.94000
LogP: 1.70320

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