Stoichiometry of the reaction of diphenylchlorophosphine with dimethylformamide in the presence of NaI
Stoichiometric relations of initial compounds and reaction products in the synthesis of N,N-dialkyl-(diphenylphosphinomethylene)iminium are established; the second reaction product is diphenylphosphinic iodide. Bringing triphenylphosphine into the reaction increases the N,N- dialkyl(diphenylphosphinomethylene)-iminium yield approximately twice. One of the reaction intermediates is shown to be iododiphenylphosphine. The reaction can be regarded as disproportionation.
Morgalyuk,Petrovskii,Lysenko,Nifant'Ev
experimental part
p. 100 - 105
(2010/05/01)
New synthesis of functionalized tertiary phosphines
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Nifant'ev,Morgaliuk,Petrovskii,Lyssenko
p. 2131 - 2132
(2008/09/19)
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