A CONVENIENT METHOD FOR THE SYNTHESIS OF DEOXYRIBONUCLEOSIDE 3'-HYDROGENPHOSPHONATES
Appropriately protected 5'-O-dimethoxytrityldeoxyribonucleoside derivatives were converted to the corresponding 3'-hydrogenphosphonates by treatment with phosphinic acid in the presence of mesitylenedisulfonyl chloride via an oxidative phosphonylation process.
Studies on aryl H-phosphonates. I. An efficient method for the preparation of deoxyribo- and ribonucleoside 3'-H-phosphonate monoesters by transesterification of diphenyl H-phosphonate
A convenient method for the preparation of deoxyribonucleoside and ribonucleoside 3'-H-phosphonate monoesters via transesterification of diphenyl H-phosphonate with suitable protected nucleosides in pyridine is described.
Jankowska,Sobkowski,Stawinski,Kraszewski
p. 3355 - 3358
(2007/10/02)
Nucleoside H-phosphonates. 12. Synthesis of nucleoside 3'-(hydrogen-phosphonothioate) monoesters via phosphinate intermediates
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Stawinski,Thelin,Westman,Zain
p. 3503 - 3506
(2007/10/02)
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