SYNTHESIS OF 1,2-CYCLOALKANEDIOLS BY INTRAMOLECULAR TITANIUM-INDUCED PINACOL COUPLING
Seven representative 1,2-cycloalkanediols of ring size 6-14 were prepared in high yield by titanium-induced pinacol coupling of dialdehydes.Cis stereochemistry predominated in six- and eight-membered rings, but trans products were formed in ring sizes ten and above.
McMurry, John E.,Rico, Joseph G.
p. 1169 - 1172
(2007/10/02)
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