The complete 1H and 13C NMR assignment of a series of imidazobenzoxazines by a combination of one- and two-dimensional experiments (COSY, HSQC and HMBC) is studied. Moreover, 2D NOESY and 1D selective NOESY are reported. This procedure allows the identification of the regioisomers obtained. Copyright
Microwave assisted efficient synthesis of imidazole-based privileged structures
A simple and efficient microwave assisted synthesis of imidazobenzoxazines, imidazobenzoxazin-5-ones, and imidazobenzoxazin-5-thiones with broad chemistry scope is described. The molecules were prepared both under conventional, as well as microwave heating conditions, to provide in high yields with clean and scalable reactions a small library of imidazole-based privileged structures for drug discovery.
Fantini, Marco,Zuliani, Valentina,Spotti, Mario A.,Rivara, Mirko
experimental part
p. 181 - 185
(2010/10/19)
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