- Rapid and convenient one-pot method for the preparation of alkali metal phosphinodiselenoates
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Alkali metal phosphinodiselenoates, R2PSe2M (R=aralkyl, hetaralkyl, Ph; M=Li, Na, K, Rb, Cs), were synthesized in high yields (up to 98%) by a three-component reaction of a secondary phosphine, elemental selenium, and an alkali metal hydroxide under mild conditions (ethanol, room temperature, 5 min). Georg Thieme Verlag Stuttgart · New York.
- Artemev, Alexander V.,Malysheva, Svetlana F.,Gusarova, Nina K.,Trofimov, Boris A.
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experimental part
p. 2463 - 2467
(2010/09/06)
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- Reaction of secondary phosphine selenides with the system Se/MOH (M = Li, Na, K, Rb, Cs): A novel three-component synthesis of diorganodiselenophosphinates
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Secondary phosphine selenides, R2P(Se)H (R = PhCH2CH2, PhCH(Me)CH2, 4-t-BuC6H4CH2CH2, NaphthylCH2CH2, Ph), react with the system Se/MOH (M = Li,
- Trofimov, Boris A.,Artem'ev, Alexander V.,Malysheva, Svetlana F.,Gusarova, Nina K.
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experimental part
p. 4116 - 4120
(2010/03/04)
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