Synthesis of 2-substituted morpholines from dihydroxyalkylsulfamates
2-Substituted morpholines and hexahydro-1,4-oxazepines were prepared by cyclodehydration of potassium dihydroxyalkylsulfamates in concentrated sulfuric acid.
Bulatov,Ermakov,Tartakovsky
p. 2100 - 2102
(2007/10/03)
Chemical Properties
Boiling Point: 198.8 °C at 760 mmHg
Flash Point:74 °C
Density: 0.931 g/cm3
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C
