- Efficient synthesis of heterophosphole-2-sulfides by solvent-free microwave reaction
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Microwave irradiation of a stoichiometric amount of Lawesson's reagent in the presence of o-aminophenols, o-aminothiophenols, o-phenylenediamines, or catechols leads to benzoxazaphosphole-, benzothiazaphosphole-, benzodiazaphosphole-, and benzodioxaphosphole-2-sulfides, respectively, in good yields in a fast and direct way under solventless conditions. The procedure requires short reaction times and is similar for all reagents; thus it may be used in parallel synthesis.
- Seijas, Julio A.,Vázquez-Tato, M. Pilar,Crecente-Campo, José
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