Synthesis and Properties of Trimethyl(trifluorosilyl)stannane
Trimethyltin hydride reacts with SiF3SiF3 or SiF3SiF2H to give the new compound SnMe3(SiF3) in 75-80 percent yield.No reaction was observed between SnMe3H and SiF3SiH3.Hydrogen-deuterium exchange was observed between tin and silicon during the course of deuterium-labelling experiments.Dimethylstannylene (SnMe2) was implicated as an intermediate by trapping experiments in the thermolysis of SnMe3(SiF3).
D'Errico, John,Sharp, Kenneth G.
p. 1879 - 1882
(2007/10/02)
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