Ceric ammonium nitrate-mediated detritylation of tritylated amines
Efficient deprotection of tritylated amines to the corresponding amines mediated by 20 mol % ceric ammonium nitrate [Ce(NH4) 2(NO3)6, CAN], 10 equiv of acetic acid and 15 equiv of water in dichloromethane is presented. This method equally worked well in the case of morpholino nucleosides.
Pattanayak, Sankha,Sinha, Surajit
supporting information; experimental part
p. 34 - 37
(2011/02/25)
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