Fluoro-Substituted Methyllithium Chemistry: External Quenching Method Using Flow Microreactors
The external quenching method based on flow microreactors allows the generation and use of short-lived fluoro-substituted methyllithium reagents, such as fluoromethyllithium, fluoroiodomethyllithium, and fluoroiodostannylmethyllithium. Highly chemoselective reactions have been developed, opening new opportunities in the synthesis of fluorinated molecules using fluorinated organometallics.
A convenient quick synthesis of SnBu2RCl derivatives
A convenient method for the quick preparation of SnBu2RX (Bu = n-Bu) has been developed using microwave irradiation and column chromatography in acidic alumina. The method can be a good alternative particularly for easy and quick preparation of
Carrera, Nora,Monica,Perez-Temprano,Albeniz, Ana C.,Casares, Juan A.,Espinet, Pablo
p. 3957 - 3958
(2009/12/08)
Group 4 Organometallic Compounds. Part 8. Preparation and Moessbauer Spectra of Five- and Six-co-ordinate Di- and Tri-organotin Compounds containing Mixed Phenyl and Butyl Groups on Tin
Moessbauer spectroscopic data and preparative details are reported for a range of IVBuPh>, IVBu2Ph>, and IVBuPh2> compounds.The stereochemical preferences of the butyl and phenyl groups in octahedral and trigonal-
Das, V. G. Kumar,Weng, Ng Seik,Smith, Peter J.,Hill, Robin
p. 552 - 558
(2007/10/02)
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