An efficient, continuous flow technique for the chemoselective synthesis of thioacetals
By optimizing a reagent's residence time within a packed-bed reactor, it is possible to overcome selectivity issues frequently encountered in stirred reaction vessels. This important feature is demonstrated for the chemoselective protection of 4-acetylben
Thioacetalization of carbonyl compounds by zeolite HSZ-360 as a new, effective heterogeneous catalyst
Thioacetal can be efficiently obtained at room temperature by simply dissolving the appropriate carbonyl compounds and 1,2-ethanedithiol, in dichloromethane, with zeolite HSZ-360 as a new heterogeneous catalyst. Satisfactory to good yields are obtained ev
Ballini, Roberto,Barboni, Luciano,Maggi, Raimondo,Sartori, Giovanni
p. 767 - 772
(2007/10/03)
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