Preparation and reactions of 2,4,6-tris(trifluoromethyl)phenylamine
Starting from RfH (1) [Rf = 1,3,5-tris(trifluoromethyl)phenyl] RfNH2 (6) is obtained in a four-step synthesis. The amine 6 reacts with chlorotrimethylsilane in the presence of DBU (1,8-diazabicyclo(5,4,0)undec-7
Ahlemann, Jens-T,Roesky, Herbert W.,Noltemeyer, Mathias,Schmidt, Hans-G.,Markovsky, Leonid N.,Shermolovich, Yuri G.
p. 87 - 90
(2007/10/03)
New Aspects of the Chemistry of 2,4,6-Tris(trifluoromethyl) Benzoic Acid and Related Compounds
1,3,5-Tris(trifluoromethyl)benzene reacts with n-butyllithium and carbon dioxide to give a high yield of 2,4,6-tris(trifluoromethyl)benzoic acid.The acid has been well characterized by spectral and pKa data.The acid chloride is formed only slow
Filler, Robert,Gnandt, William K.,Chen, Wei,Lin, Shan
p. 99 - 105
(2007/10/02)
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