Synthesis and Photolysis of N-(Phenoxycarbonyloxy)-2-thiopyridone Derivatives. A New Unimolecular Route to Quantitative Generation of Phenoxyl Radicals
N-(Phenoxycarbonyloxy)-2-thiopyridone derivatives were prepared by the reaction of lithium phenoxides with phosgene followed by the reaction with 2-mercaptopyridine N-oxide and photolyzed to give quantitative yield of phenoxyl radicals.
Togo, Yoshifumi,Nakamura, Nobuo,Iwamura, Hiizu
p. 1201 - 1204
(2007/10/02)
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