- Systematic comparison of sets of 13C NMR spectra that are potentially identical. Confirmation of the configuration of a cuticular hydrocarbon from the cane beetle antitrogus parvulus
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A systematic process is introduced to compare 13C NMR spectra of two (or more) candidate samples of known structure to a natural product sample of unknown structure. The process is designed for the case where the spectra involved can reasonably
- Basar, Norazah,Damodaran, Krishnan,Liu, Hao,Morris, Gareth A.,Sirat, Hasnah M.,Thomas, Eric J.,Curran, Dennis P.
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p. 7477 - 7490
(2014/10/15)
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- Total synthesis of a cuticular hydrocarbon from the cane beetle Antitrogus parvulus: Confirmation of the relative stereochemistry
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The stereoselective reaction of an allyl bromide with an aldehyde mediated by a low valency bismuth species was the key reaction in stereoselective syntheses of (4S,6R,8R,10S,16S)- and (4S,6R,8R,10S,16R)-4,6,8,10,16- pentamethyldocosanes. 13C N
- Basar, Norazah B.,Liu, Hao,Negi, Devendra,Sirat, Hasnah M.,Morris, Gareth A.,Thomas, Eric J.
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p. 1743 - 1745
(2012/04/23)
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