- Synthesis and characterisation of medium-sized ring systems by oxidative cleavage. Part 2: Insights from the study of ring expanded analogues
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Variable temperature NMR analysis and computational methods have been used to develop a detailed understanding of the 1H NMR spectra of a family of medium-sized ring containing compounds. The family consists of analogues containing 10-, 11- and
- Lebl, Tomas,Lorion, Magali M.,Jones, Alan M.,Philp, Douglas,Westwood, Nicholas J.
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experimental part
p. 9694 - 9702
(2011/02/23)
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- The chemical reactivity of a known anti-psoriasis drug. Part 1: Further insights into the products resulting from oxidative cleavage
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The oxidative cleavage of the known anti-psoriasis drug 1 to give 2 has been reported previously. Due to the importance of accessing medium-sized ring containing systems via oxidative cleavage, this reaction has been revisited revealing additional informa
- Jones, Alan M.,Lorion, Magali M.,Lebl, Tomas,Slawin, Alexandra M.Z.,Philp, Douglas,Westwood, Nicholas J.
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experimental part
p. 9667 - 9674
(2011/02/25)
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- Oxidative Cleavage of a Tricyclic Pyridone to a Bicyclic Lactam-dione
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Two equivalents of anhydrous m-chloroperbenzoic acid (m-CPBA) cleaved the pyridone ring of 10-(3-chlorophenyl)-6,8,9,10-tetrahydrobenzonaphthyridin-5(7H)-one, forming the ten-membered lactam α-diketone 12-(3-chlorophenyl)-7,8,9,10-tetrahydropyrido
- Friary, Richard J.,Schwerdt, John H.
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p. 9981 - 9984
(2007/10/02)
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