Synthesis and reactions of 4-sulpho-2,3,5,6-tetrafluorobenzoic acid
4-Sulpho-2,3,5,6-tetrafluorobenzoic acid (I) has been synthesised from pentafluorobenzoic acid via the oxidation of 4-mercapto-tetrafluorobenzoic acid.Reaction of I with DMF/SOCl2 gave 1,4-ClC6F4COCl (IIA) which was converted to 1,4-ClC6F4COF (IIB) by flu
Fielding, H. C.,Shirley, I. M.
p. 15 - 31
(2007/10/02)
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