cas 145788-51-8, Ethanone, 1-(3-hydroxy-1-cyclohexen-1-yl)-, (R)- (9CI) | Articles data ｜lookchem

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145788-51-8

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Total synthesis of (+)-compactin by a double Michael protocol
The total synthesis of (+)-compactin 1 has been achieved by employing a double Michael reaction of (R)-1-acetyl-3-(tert-butyldimethylsiloxy)cyclohexene 16 with methyl crotonate as the key reaction.
Hagiwara, Hisahiro,Nakano, Takashi,Kon-no, Masakazu,Uda, Hisashi
p. 777 - 784
(2007/10/02)

A Novel Synthesis Including Asymmetric Synthesis of α,β-Unsaturated γ-Hydroxy Carbonyl Compounds from Enones with Carbon Homologation
Reaction of the carbanion derived from 1-chloroalkyl aryl sulfoxides with enones gave 1,2-adducts in good yields.Treatment of the adduct with potassium benzenethiolate afforded α-phenylthio β,γ-unsaturated carbonyl compound through an α,β-epoxy sulfoxide.
Satoh, Tsuyoshi,Motohashi, Shigeyasu,Tokutake, Norio,Yamakawa, Koji
p. 2966 - 2973
(2007/10/02)

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Chemical Properties

Boiling Point: 271.6±40.0 °C(Predicted)
Density: 1.112±0.06 g/cm3(Predicted)
PKA: 14.32±0.40(Predicted)
PSA: 37.30000
LogP: 1.04660

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