Syntheses of 1,2-Thiaphospholes and Their Thermal and Lewis Acid-Promoted Addition Reactions
3,5-Di-substituted 1,2-thiaphospholes were efficiently prepared by treating 2,9-dithia-1-phosphabicyclo-nona-3,7-diene 1-sulfides with n-Bu3P.The thiaphospholes reacted thermally with norbornadiene, norbornene or dietyl azodicarboxylate to produce
Shinoda, Ikuo,Takahashi, Akihiko,Saito, Takao,Uchida, Tokiko
p. 2785 - 2794
(2007/10/02)
Preparation and Reactions of 1,2-Thiaphospholes
Treatment of 2,9-dithia-1-phosphabicyclo-nona-3,7-diene 1-sulfides with n-Bu3P afforded 1,2-thiaphospholes in good yields.The thiaphospholes reacted thermally with norbornene to produce 1:2 double Diels-Alder cycloadducts, whereas they reacted with
Motoki, Shinichi,Sakai, Takaya,Shinoda, Ikuo,Saito, Takao,Uchida, Tokiko
p. 1563 - 1566
(2007/10/02)
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