cas 163125-34-6, 1,1,2,2-TETRAMETHOXYCYCLOHEXANE | Articles data ｜lookchem

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163125-34-6

Articles about 163125-34-6Total 4 be found

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Synthesis of bridged head methyl 3,4-O-(1',2'-dimethylcycloheaxane- 1',2'-diyl)-6,7-dideoxy-α-D-mannooct-6-ene-pyranose-8,2-lactone from D- mannose
The vicinal diequatorial diol at C-3 and C-4 of (1) was masked as cyclohexane diacetal derivative (2). Selective protection of C-2 as benzyl ether (3a) and Swern oxidation of the primary 6-OH gave the aldehyde derivative (4). Stereoselective Wittig condensation of (4) with Ph3P=CH- CO2Me followed by debenzylation and cyclization afforded the bridged α,β- unsaturated lactone derivative (8) in a moderate overall yield.
Hassan, Hammed H. A. M.
p. 397 - 407
(2007/10/03)

(1′S,2′S)-methyl-3O,4O-(1′,2′-dimethoxycyclohexane-1′,2′-diyl)-α-D-mannopyranoside [α-D-Mannopyranoside, methyl 3,4-O-(1,2-dimethoxy- 1,2-cyclohexanediyl)-, [3[S (S)]]-]
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Ley, Steven V.,Osborn, Helen M. I.,Priepke, Henning W. M.,Warriner, Stuart L.,Scheidt, Karl A.,Roush, William R.
p. 170 - 170
(2017/09/30)

Preparation, structure, derivatisation and NMR data of cyclohexane-1,2-diacetal protected carbohydrates
Acid catalysed reaction of monosaccharides with 1,1,2,2-tetramethoxycyclohexane results in selective protection of vicinal, diequatorial, diol functionality as a cyclohexane-1,2-diacetal (CDA). This new methodology complements classical cyclic acetal prot
Grice, Peter,Ley, Steven V.,Pietruszka, Joerg,Priepke, Henning W. M.,Warriner, Stuart L.
p. 351 - 363
(2007/10/03)

Cyclohexan-1,2-diacetale (CDA): eine neue Schutzgruppe fuer vicinale Diole in Kohlenhydraten
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Ley, Steven V.,Priepke, Henning W. M.,Warriner, Stuart L.
p. 2410 - 2412
(2007/10/02)

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Chemical Properties

Appearance/Colour :Clear yellow to brown-yellow liquid
Boiling Point: 224.2 °C at 760 mmHg
Flash Point:70.1 °C
Density: 1.01 g/cm³
Storage Temp.:0-6°C
Vapor Pressure: 0.138mmHg at 25°C
Refractive Index: 1.454-1.46
PSA: 36.92000
LogP: 1.53860

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