cas 174004-17-2, CYCLOHEXANONE O-PROP-2-YNYL-OXIME

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174004-17-2

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Synthesis of ketone O-allyloximes and O-propargyloximes in KOH-DMSO system
In reaction of ketone oximes with allyl bromide and propargyl chloride in KOH - DMSO system were obtained in good yield previously unknown ketone O-allyloximes and O-propargyloximes. The reactions are accompanied with minor regeneration of ketones (up to 12%, mainly 1-5%).
Tarasova,Shmidt,Sinegovskaya,Petrova,Sobenina,Mikhaleva,Brandsma,Trofimov
p. 1581 - 1586
(2007/10/03)

The Base-Catalysed Rearrangement of O-Propargyl Ketoximes to N-1-Alkenyl Acryl Amides
O-Propargyl ketoximes, available from the reaction of ketoximes with propargyl halides in KOH/DMSO system, readily undergo base-catalysed (t-BuOK in DMSO or THF) rearrangement to N-(1-alkenyl)acrylamides in 15-58percent yields.
Trofimov, Boris A.,Tarasova, Ol'ga A.,Sigalov, Mark V.,Mikhaleva, Al'bina I.
p. 9181 - 9184
(2007/10/02)

Chemical Properties

Boiling Point: 217°Cat760mmHg
Flash Point:72.4°C
Density: 0.95g/cm³
Vapor Pressure: 0.199mmHg at 25°C
Refractive Index: 1.486
PSA: 21.59000
LogP: 1.95630

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174004-17-2

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Chemical Properties

Boiling Point: 217°Cat760mmHg

Flash Point:72.4°C

Density: 0.95g/cm³

Vapor Pressure: 0.199mmHg at 25°C

Refractive Index: 1.486

PSA: 21.59000

LogP: 1.95630

Global suppliers and manufacturers of 174004-17-2total 2 suppliers on LookChem

Article Database

174004-17-2

Articles about 174004-17-2Total 2 be found

More Articles about upstream products of 174004-17-2

Chemical Properties

Boiling Point: 217°Cat760mmHg

Flash Point:72.4°C

Density: 0.95g/cm3

Vapor Pressure: 0.199mmHg at 25°C

Refractive Index: 1.486

PSA: 21.59000

LogP: 1.95630

Global suppliers and manufacturers of 174004-17-2total 2 suppliers on LookChem

Density: 0.95g/cm³