cas 2106-02-7, 2-Chloro-4-fluoroaniline | Articles data ｜lookchem

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2106-02-7

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Mulvey et al.
p. 1419
(1978)
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Preparation of fully substituted anilines for the synthesis of functionalized indoles
A wide range of highly functionalized indoles were prepared by the successive magnesiation of readily available o-alkynyl protected anilines using TMPMgCl·LiCl or LDA, followed by a KH-mediated cyclization reaction.
Stoll, Armin H.,Knochel, Paul
p. 113 - 116
(2008/04/12)

The Bamberger reaction in hydrogen fluoride: the use of mild reductive metals for the preparation of fluoroaromatic amines
The reduction of nitroaromatic compounds by various metals (tin, lead, bismuth) in liquid hydrogen fluoride under an inert atmosphere leads to fluoroaromatic amines, in accord with the Bamberger reaction.Generally, a co-solvent such as pentane or methylene chloride is used.Some non-fluorinated arylamines are also formed by a competitive direct reduction of the N-arylhydroxylamine intermediate.Of the mild reductive metals studied, bismuth was the most selective. - Keywords: Bamberger reaction; Hydrogen fluoride; Mild reductive metals; Fluoroaromatic amines; NMR spectroscopy
Tordeux, Marc,Wakselman, Claude
p. 251 - 254
(2007/10/03)

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Chemical Properties

Appearance/Colour :clear orange-brown to brown liquid
Melting Point: 192oC(lit.)
Boiling Point: 192 °C at 760 mmHg
Flash Point:98.3 °C
Density: 1.219 g/cm³
Storage Temp.:Room temperature.
Vapor Pressure: 0.5mmHg at 25°C
Refractive Index: n20/D 1.554(lit.)
PKA: 2.71±0.10(Predicted)
BRN: 2802559
PSA: 26.02000
LogP: 2.64250

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