Substituent-controlled, mild oxidative fluorination of iodoarenes: Synthesis and structural study of aryl I(iii)- and I(v)-fluorides
We report a mild approach to the synthesis of difluoro(aryl)-λ3-iodanes (aryl-IF2 compounds) and tetrafluoro(aryl)-λ5-iodanes (aryl-IF4 compounds) using trichloroisocyanuric acid (TCICA) and potassium fluoride (
H?fliger, Joel,Pitts, Cody Ross,Bornemann, Dustin,K?ser, Roland,Santschi, Nico,Charpentier, Julie,Otth, Elisabeth,Trapp, Nils,Verel, René,Lüthi, Hans Peter,Togni, Antonio
p. 7251 - 7259
(2019/08/07)
Phenyliodine(V) fluorides
The known compound phenyltetrafluoroiodine(V) is shown by X-ray diffraction to have a tetragonal pyramidal structure with an apical phenyl group. This structure is compared to that of IF(OTeF5)4, where the apical position is occupied
Hoyer, Sevim,Seppelt, Konrad
p. 989 - 996
(2007/10/03)
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