Synthesis of fluazolate via the application of regioselective [3+2] cyclocondensation and nucleophilic substitution-cyclization strategies
Starting from commercially available 2-chloro-4-fluorobenzoic acid 4, synthesis of fluazolate was achieved in up to 30% overall yield via the key procedure of either regioselective [3+2] cyclocondensation of trifluoromethyl-α,β-ynone 2 with hydrazine hydr
Hsieh, Min-Tsang,Lin, Hui-Chang,Kuo, Sheng-Chu
p. 5880 - 5885
(2016/09/07)
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