cas 38338-20-4, 4-bromo-6-chlorobenzo[d]thiazol-2-amine | Articles data ｜lookchem

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38338-20-4

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PBr3-mediated unexpected reductive deoxygenation of α-aryl-pyridinemethanols: Synthesis of arylmethylpyridines
PBr3-mediated reductive deoxygenation of α-aryl-pyridinemethanols to provide arylmethylpyridines is described, the alcohol substrate scope is explored, free radical trap TEMPO (2,2,6,6-tetramethyl-1-piperidinyloxy) is introduced, and the hydrogen source of the methylene product is defined. The unexpected reaction enabled us to prepare previously inaccessible, novel EP1 antagonists.
Nishigaya, Yosuke,Umei, Kentaro,Watanabe, Daisuke,Kohno, Yasushi,Seto, Shigeki
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p. 1566 - 1572
(2016/03/01)

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Chemical Properties

Melting Point: 210 °C(Solv: ethanol (64-17-5))
Boiling Point: 395.6°C at 760 mmHg
Flash Point:193°C
Density: 1.928g/cm³
Vapor Pressure: 1.82E-06mmHg at 25°C
Refractive Index: 1.78
PKA: 1.50±0.10(Predicted)
PSA: 67.88000
LogP: 3.22450

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